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三乙酰氧基乙烯基硅烷

产品名称 三乙酰氧基乙烯基硅烷

CAS号4130-08-9

分子式C8H12O6Si

分子量232.26

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  • Mass

    MS-NW-8335          
    triacetoxyvinylsilane
    C8H12O6Si           (Mass of molecular ion:    232)
    

       Source Temperature: 260 °C
       Sample Temperature: 140 °C
       Reservoir, 75 eV
    

          13.0       1.1
          14.0       4.1
          15.0      16.9
          16.0       1.8
          27.0       1.7
          28.0       7.5
          29.0       3.2
          41.0       1.7
          42.0      11.2
          43.0      89.7
          44.0       3.0
          45.0      34.6
          60.0      22.5
          61.0       1.3
          62.0       5.3
          63.0      14.8
          76.0       4.5
          79.0      30.1
          80.0       1.6
          81.0       1.2
          87.0       2.9
          88.0       3.0
          89.0      39.9
          90.0       3.2
          91.0       1.8
         102.0       1.3
         103.0       1.2
         104.0       5.1
         105.0       2.5
         118.0       1.0
         120.0       1.0
         121.0     100.0
         122.0       7.6
         123.0       5.6
         129.0       1.1
         130.0      11.1
         131.0      51.5
         132.0       5.4
         133.0       4.4
         139.0       1.2
         146.0       1.5
         147.0       5.7
         148.0       3.6
         149.0       2.2
         163.0      55.5
         164.0       5.4
         165.0       2.9
         167.0       1.1
         172.0       7.2
         173.0       9.2
         174.0       1.5
         175.0       3.1
         177.0       1.5
         189.0       3.7
         190.0       1.3
         191.0       1.1
         205.0      35.5
         206.0       4.3
         207.0       2.1
         209.0       3.6
         217.0       1.7
         218.0       3.0
         219.0       2.6
         251.0       4.2
         260.0       2.0
         261.0       2.0
         293.0       3.6
         303.0       2.2
         335.0       3.5
    

90 MHz in CDCl3

parameter in CDCl3


  • 1H NMR 89.56 MHz
    C8 H12 O6 Si 0.04 ml : 0.5 ml CDCl3
    triacetoxyvinylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.38 to 6.04 B 2.161

         Hz     ppm     Int.
    

        570.06   6.366     37
        562.13   6.277     71
        558.56   6.237     88
        555.44   6.202     80
        547.50   6.114     39
        193.56   2.162   1000
        189.88   2.121     41
    


  • 1H NMR 300 MHz
    C8 H12 O6 Si 0.05 ml : 0.5 ml CDCl3
    triacetoxyvinylsilane
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 6.344 D(B) 6.224 D(C) 6.110 J(A,B) 3.0 J(A,C) 15.4 J(B,C) 18.6 D(D) 2.163

         Hz     ppm     Int.
    

       1913.35   6.378     21
       1909.33   6.364     23
       1898.96   6.330     29
       1894.94   6.316     38
       1880.78   6.269     12
       1876.80   6.256     17
       1862.21   6.207     50
       1858.23   6.194     34
       1846.32   6.154     51
       1831.89   6.106     31
       1827.75   6.092     16
       1813.36   6.045     13
        648.91   2.163   1000
    

in CDCl3



CCl4 solution



liquid film