-
MassMS-NW-5997 2,8-decadiyne C10H14 (Mass of molecular ion: 134)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
26.0 2.2 27.0 35.5 29.0 5.1 38.0 3.3 39.0 40.1 40.0 10.0 41.0 55.5 42.0 3.8 50.0 8.8 51.0 21.8 52.0 13.8 53.0 73.2 54.0 9.9 55.0 16.6 56.0 1.8 62.0 2.2 63.0 5.5 64.0 2.1 65.0 19.5 66.0 15.7 67.0 25.8 68.0 16.4 69.0 2.5 74.0 1.2 75.0 1.0 77.0 46.7 78.0 13.1 79.0 54.9 80.0 8.1 81.0 5.8 82.0 1.8 89.0 1.1 91.0 100.0 92.0 15.0 93.0 13.2 94.0 3.4 95.0 1.9 103.0 9.2 104.0 7.4 105.0 48.6 106.0 55.3 107.0 6.4 115.0 4.4 116.0 1.9 117.0 12.5 118.0 2.9 119.0 82.9 120.0 8.7 131.0 1.6 133.0 12.5 134.0 1.9
400 MHz in CDCl3
-
1H NMR 399.65 MHz C10 H14 0.04 ml : 0.5 ml CDCl3 2,8-decadiyne 
Assign. Shift(ppm)
A 2.143 B 1.777 C 1.567
Hz ppm Int.864.50 2.164 54 863.16 2.160 46 861.82 2.157 74 860.11 2.153 90 858.76 2.149 78 857.54 2.146 159 856.32 2.143 89 854.98 2.140 159 853.76 2.137 79 852.42 2.133 89 850.83 2.129 71 849.49 2.126 43 848.14 2.123 52 714.97 1.789 46 712.65 1.784 583 710.21 1.778 1000 707.52 1.771 502 635.38 1.590 32 632.57 1.583 104 631.47 1.581 71 629.52 1.576 90 628.78 1.574 111 626.95 1.569 71 625.85 1.566 329 622.80 1.559 99 621.95 1.557 88 620.12 1.552 59 618.90 1.549 86
in CDCl3
liquid film
4880 A,200 M,liquid
更多供应商
