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MassMS-NW-9674 tris(2-aminoethyl)amine C6H18N4 (Mass of molecular ion: 146)
Source Temperature: 270 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.7 16.0 1.0 17.0 2.4 18.0 15.4 27.0 3.3 28.0 9.0 29.0 2.1 30.0 16.4 40.0 1.0 41.0 3.7 42.0 13.4 43.0 9.1 44.0 100.0 45.0 4.2 54.0 1.2 55.0 1.5 56.0 29.3 57.0 3.3 58.0 13.7 59.0 1.8 68.0 2.6 69.0 2.5 70.0 19.2 71.0 4.9 72.0 2.2 73.0 29.9 74.0 1.3 79.0 1.0 81.0 1.2 82.0 1.6 83.0 1.8 84.0 5.0 85.0 9.6 87.0 13.5 91.0 1.3 97.0 5.8 98.0 2.7 99.0 74.0 100.0 5.4 112.0 2.2 116.0 73.7 117.0 5.0 127.0 1.3 130.0 1.1 147.0 3.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H18 N4 0.05 ml : 0.5 ml CDCl3 tris(2-aminoethyl)amine 
Assign. Shift(ppm)
A 2.745 B 2.521 C 1.36
Hz ppm Int.262.19 2.928 30 254.38 2.841 189 252.50 2.820 217 249.13 2.782 273 246.88 2.757 557 242.06 2.703 539 241.13 2.693 540 236.31 2.639 51 236.19 2.638 51 230.50 2.574 550 229.56 2.564 510 224.81 2.511 528 222.50 2.485 242 219.13 2.447 200 217.19 2.426 164 215.31 2.405 34 121.56 1.358 1000
in CDCl3
liquid film
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