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MS-IW-3456 2-methoxyacetophenone C9H10O2 (Mass of molecular ion: 150)
Source Temperature: 210 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 1.3 29.0 2.1 39.0 1.8 45.0 9.8 50.0 4.6 51.0 13.4 63.0 1.1 65.0 1.9 74.0 1.6 75.0 1.1 76.0 2.3 77.0 54.9 78.0 4.2 91.0 3.5 105.0 100.0 106.0 8.5 120.0 20.9 121.0 2.0 153.0 1.1 154.0 3.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H10 O2 0.05 ml : 0.5 ml CDCl3 2-methoxyacetophenone Assign. Shift(ppm)
A 7.912 B 7.565 C 7.449 D 4.702 E 3.493
Hz ppm Int.
3168.58 7.929 42 3166.75 7.924 194 3166.14 7.923 152 3165.41 7.921 237 3164.79 7.919 108 3164.31 7.918 96 3163.70 7.917 86 3160.40 7.908 79 3158.33 7.903 256 3156.98 7.900 247 3032.71 7.589 47 3031.37 7.586 90 3030.03 7.582 48 3025.88 7.572 59 3024.66 7.569 92 3023.93 7.567 143 3022.09 7.562 64 3017.82 7.552 76 3016.48 7.548 124 3015.26 7.545 70 2986.21 7.473 52 2984.99 7.470 153 2984.50 7.468 182 2983.89 7.467 111 2982.91 7.464 96 2977.66 7.451 135 2976.93 7.449 201 2976.56 7.448 231 2976.07 7.447 178 2975.22 7.445 89 2973.63 7.441 35 2970.95 7.434 64 2969.73 7.431 76 2969.24 7.430 144 2968.51 7.428 106 2967.65 7.426 47 2966.31 7.423 36 1879.15 4.702 712 1396.12 3.494 1000
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