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MS-IW-9054 ethyl chlorofluoroacetate C4H6ClFO2 (Mass of molecular ion: 140)
Source Temperature: 200 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.1 26.0 1.7 27.0 18.0 28.0 12.3 29.0 100.0 30.0 2.4 31.0 1.9 32.0 2.3 43.0 2.0 45.0 2.4 49.0 2.8 60.0 5.0 61.0 7.0 63.0 1.0 67.0 21.4 69.0 7.2 73.0 1.3 77.0 1.4 97.0 3.8 99.0 1.2 105.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H6 Cl F O2 0.05 ml : 0.5 ml CDCl3 ethyl chlorofluoroacetate Assign. Shift(ppm)
A 6.302 B 4.355 C 1.361
Hz ppm Int.
2544.31 6.367 472 2494.02 6.241 486 1751.46 4.383 198 1747.31 4.373 29 1744.38 4.365 501 1737.18 4.347 509 1734.01 4.339 29 1729.98 4.329 205 551.27 1.380 671 548.71 1.373 34 544.19 1.362 1000 541.02 1.354 51 538.82 1.349 37 536.99 1.344 645
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