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网站主页CAS数据库列表 401-56-9更多图谱氯氟乙酸乙酯(401-56-9)核磁图(13CNMR)

氯氟乙酸乙酯

产品名称 氯氟乙酸乙酯

CAS号401-56-9

分子式C4H6ClFO2

分子量140.54

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  • Mass

    MS-IW-9054          
    ethyl chlorofluoroacetate
    C4H6ClFO2           (Mass of molecular ion:    140)
    

       Source Temperature: 200 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       1.1
          26.0       1.7
          27.0      18.0
          28.0      12.3
          29.0     100.0
          30.0       2.4
          31.0       1.9
          32.0       2.3
          43.0       2.0
          45.0       2.4
          49.0       2.8
          60.0       5.0
          61.0       7.0
          63.0       1.0
          67.0      21.4
          69.0       7.2
          73.0       1.3
          77.0       1.4
          97.0       3.8
          99.0       1.2
         105.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C4 H6 Cl F O2 0.05 ml : 0.5 ml CDCl3
    ethyl chlorofluoroacetate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.302 B 4.355 C 1.361

         Hz     ppm     Int.
    

       2544.31   6.367    472
       2494.02   6.241    486
       1751.46   4.383    198
       1747.31   4.373     29
       1744.38   4.365    501
       1737.18   4.347    509
       1734.01   4.339     29
       1729.98   4.329    205
        551.27   1.380    671
        548.71   1.373     34
        544.19   1.362   1000
        541.02   1.354     51
        538.82   1.349     37
        536.99   1.344    645
    

in CDCl3



liquid film