(甲氧基甲基)三苯基氯化磷

Mass

MS-IW-0037          
(methoxymethyl)triphenylphosphonium chloride
C20H20ClOP          (Mass of molecular ion:    342)

   Source Temperature: 210 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      15.0       1.0
      29.0       1.3
      45.0       5.9
      49.0       1.0
      51.0       1.5
     107.0       6.0
     108.0      22.7
     109.0       1.7
     115.0       1.3
     131.0       1.2
     133.0       1.3
     152.0       4.4
     153.0       1.0
     157.0       2.0
     170.0       1.2
     183.0      41.5
     184.0      12.1
     185.0       6.4
     261.0      16.2
     262.0     100.0
     263.0      19.4
     264.0       1.8

Assign. Shift(ppm) A 7.84 B 7.82 C 7.721 D 5.841 E 3.715

     Hz     ppm     Int.

   3143.19   7.865     59
   3141.85   7.862    122
   3139.89   7.857    152
   3137.45   7.851    312
   3136.23   7.848    367
   3134.64   7.844    489
   3132.57   7.839    357
   3130.98   7.835    270
   3128.30   7.828    559
   3127.44   7.826    468
   3124.76   7.819    401
   3123.78   7.817    420
   3118.41   7.803    155
   3116.33   7.798    490
   3114.87   7.794    362
   3094.12   7.743    354
   3090.58   7.734    387
   3086.67   7.724    379
   3083.13   7.715    414
   3078.86   7.704    208
   3076.78   7.699    115
   3075.20   7.695    182
   2336.55   5.847    381
   2332.52   5.837    402
   1485.11   3.717   1000
   1484.38   3.715    949