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MS-IW-0037 (methoxymethyl)triphenylphosphonium chloride C20H20ClOP (Mass of molecular ion: 342)
Source Temperature: 210 °C Sample Temperature: 170 °C Direct, 75 eV
15.0 1.0 29.0 1.3 45.0 5.9 49.0 1.0 51.0 1.5 107.0 6.0 108.0 22.7 109.0 1.7 115.0 1.3 131.0 1.2 133.0 1.3 152.0 4.4 153.0 1.0 157.0 2.0 170.0 1.2 183.0 41.5 184.0 12.1 185.0 6.4 261.0 16.2 262.0 100.0 263.0 19.4 264.0 1.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C20 H20 Cl O P 0.037 g : 0.5 ml CDCl3 (methoxymethyl)triphenylphosphonium chloride Assign. Shift(ppm)
A 7.84 B 7.82 C 7.721 D 5.841 E 3.715
Hz ppm Int.
3143.19 7.865 59 3141.85 7.862 122 3139.89 7.857 152 3137.45 7.851 312 3136.23 7.848 367 3134.64 7.844 489 3132.57 7.839 357 3130.98 7.835 270 3128.30 7.828 559 3127.44 7.826 468 3124.76 7.819 401 3123.78 7.817 420 3118.41 7.803 155 3116.33 7.798 490 3114.87 7.794 362 3094.12 7.743 354 3090.58 7.734 387 3086.67 7.724 379 3083.13 7.715 414 3078.86 7.704 208 3076.78 7.699 115 3075.20 7.695 182 2336.55 5.847 381 2332.52 5.837 402 1485.11 3.717 1000 1484.38 3.715 949
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