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MassMS-NW-5449 ethyl (3-pyridyl)acetate C9H11NO2 (Mass of molecular ion: 165)
Source Temperature: 240 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.0 18.0 1.4 26.0 2.0 27.0 8.2 28.0 2.5 29.0 53.0 30.0 1.3 31.0 1.0 37.0 1.2 38.0 4.4 39.0 24.7 40.0 1.6 45.0 1.0 46.0 1.1 50.0 1.2 51.0 1.7 52.0 1.4 53.0 1.1 62.0 1.8 63.0 6.4 64.0 5.4 65.0 27.0 66.0 3.7 80.0 1.1 91.0 4.1 92.0 100.0 93.0 36.1 94.0 2.4 106.0 2.1 108.0 1.0 119.0 1.9 120.0 6.3 121.0 10.8 122.0 1.1 137.0 1.6 165.0 35.6 166.0 4.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H11 N O2 0.04 ml : 0.5 ml CDCl3 ethyl (3-pyridyl)acetate 
Assign. Shift(ppm)
A 8.57 to 8.46 B 7.637 C 7.266 D 4.163 E 3.618 F 1.256 J(D,F)=7.2HZ. J(A,C)=4.8HZ. J(B,C)=7.9HZ.
Hz ppm Int.764.19 8.533 156 762.56 8.515 118 762.13 8.510 117 761.38 8.502 115 759.38 8.480 84 690.56 7.711 43 688.88 7.692 63 688.31 7.686 61 687.69 7.679 30 686.56 7.666 42 682.69 7.623 63 682.19 7.618 42 681.00 7.604 94 680.44 7.598 94 679.88 7.592 46 679.25 7.585 42 678.75 7.579 60 656.06 7.326 82 651.25 7.272 72 650.38 7.262 75 648.19 7.238 55 647.38 7.229 53 643.44 7.185 48 642.56 7.175 47 383.88 4.287 107 376.63 4.206 362 369.50 4.126 382 362.44 4.047 125 324.00 3.618 528 119.38 1.333 457 112.31 1.255 1000 105.13 1.174 404
in CDCl3
liquid film
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