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网站主页CAS数据库列表 39896-06-5更多图谱奎宁环盐酸盐(39896-06-5)核磁图(1HNMR)

奎宁环盐酸盐

产品名称 奎宁环盐酸盐

CAS号39896-06-5

分子式C7H14ClN

分子量147.65

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  • Mass

    MS-NW-3182          
    quinuclidine hydrochloride
    C7H13N HCl          (Mass of molecular ion:    111)
    

       Source Temperature: 220 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          15.0       3.0
          18.0       1.2
          26.0       1.0
          27.0       8.3
          28.0       5.8
          29.0       4.8
          30.0       2.0
          35.0       3.1
          36.0      27.3
          37.0       1.0
          38.0       9.0
          39.0       6.3
          40.0       1.1
          41.0      10.8
          42.0     100.0
          43.0       5.2
          44.0       1.1
          51.0       1.1
          53.0       3.7
          54.0       5.6
          55.0      20.0
          56.0       6.2
          57.0       9.6
          67.0       1.9
          68.0       5.7
          69.0      14.3
          70.0       2.9
          81.0       2.5
          82.0      37.5
          83.0      16.2
          84.0       1.6
          96.0      23.3
          97.0       1.7
         110.0      20.9
         111.0      44.7
         112.0       3.6
    

400 MHz in D2O


  • 1H NMR 399.65 MHz
    C7 H13 N 0.043 g : 0.5 ml D2O
    quinuclidine hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    B 3.320 C 2.156 D 1.940 The solvent signal removed.

         Hz     ppm     Int.
    

       1335.33   3.342    956
       1329.35   3.327    690
       1327.15   3.321    936
       1324.71   3.315    615
       1318.97   3.301   1000
        868.53   2.174    137
        865.23   2.165    342
        861.94   2.157    474
        858.64   2.149    386
        855.35   2.141    176
        784.91   1.964    569
        781.49   1.956    610
        779.66   1.951    469
        776.49   1.943    764
        773.93   1.937    716
        770.39   1.928    458
        768.55   1.924    596
        765.26   1.915    486
    

D2O



KBr disc



nujol mull



4880 A,200 M,powder