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MS-KW-0168 4-fluoro-1,2-dimethoxybenzene C8H9FO2 (Mass of molecular ion: 156)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.9 28.0 2.6 29.0 1.8 31.0 3.7 38.0 1.2 39.0 4.0 44.0 1.7 50.0 3.5 51.0 3.5 53.0 1.5 55.0 1.4 56.0 1.8 57.0 4.4 59.0 6.5 61.0 1.1 62.0 1.3 63.0 3.4 65.0 16.7 66.0 1.2 68.0 1.4 69.0 3.7 70.0 14.8 71.0 1.6 72.0 1.8 73.0 1.1 75.0 4.1 77.0 1.1 79.0 1.0 81.0 4.4 82.0 6.5 83.0 11.5 84.0 1.1 85.0 6.6 93.0 7.2 94.0 2.1 95.0 29.7 96.0 2.9 97.0 2.7 98.0 8.9 99.0 1.0 110.0 4.4 111.0 3.1 113.0 35.6 114.0 2.5 125.0 1.0 139.0 2.0 140.0 3.3 141.0 60.7 142.0 5.2 156.0 100.0 157.0 9.1 204.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H9 F O2 0.05 ml : 0.5 ml CDCl3 4-fluoro-1,2-dimethoxybenzene Assign. Shift(ppm)
A 6.765 B 6.628 C 6.578 D *1 3.842 E *1 3.833
Hz ppm Int.
2711.06 6.784 104 2705.69 6.771 107 2702.27 6.762 131 2696.90 6.749 126 2655.76 6.646 105 2652.95 6.639 133 2645.75 6.621 105 2642.82 6.613 137 2638.43 6.602 115 2635.50 6.595 86 2630.37 6.582 127 2629.64 6.580 114 2627.44 6.575 94 2626.71 6.573 89 2621.58 6.560 90 2618.65 6.553 71 1535.40 3.842 1000 1532.10 3.834 980 1526.49 3.820 41
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