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网站主页CAS数据库列表 39777-05-4更多图谱p-丁氧基苄烯-p-戊基苯胺(39777-05-4)质谱(MS)

p-丁氧基苄烯-p-戊基苯胺

产品名称 p-丁氧基苄烯-p-戊基苯胺

CAS号39777-05-4

分子式C22H29NO

分子量323.47

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  • Mass

    MS-IW-7438          
    N-(4-butoxybenzylidene)-4-pentylaniline
    C22H29NO            (Mass of molecular ion:    323)
    

       Source Temperature: 170 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          29.0       1.6
          41.0       1.5
          43.0       1.8
          65.0       1.0
          77.0       1.0
          89.0       1.0
          90.0       2.7
          91.0       1.8
         180.0       1.6
         181.0       1.0
         196.0       1.0
         209.0       1.5
         210.0      32.8
         211.0       5.3
         266.0      65.4
         267.0      16.8
         268.0       2.1
         323.0     100.0
         324.0      24.6
         325.0       3.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C22 H29 N O 0.041 g : 0.5 ml CDCl3
    N-(4-butoxybenzylidene)-4-pentylaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.383 B 7.815 C 7.177 D 7.129 E 6.954 F 4.008 G 2.605 J 1.783 K 1.619 L 1.502 M 1.33 N 0.983 P 0.895

         Hz     ppm     Int.
    

       3350.46   8.384    481
       3130.74   7.834     42
       3128.05   7.827    372
       3126.22   7.823    125
       3121.22   7.810    119
       3119.38   7.806    408
       3116.70   7.799     52
       2876.34   7.198     30
       2874.27   7.192    210
       2872.31   7.188     89
       2868.04   7.177    118
       2865.72   7.171    465
       2854.00   7.142    100
       2852.05   7.137    562
       2849.85   7.131    143
       2845.58   7.121     99
       2843.51   7.116    261
       2841.55   7.111     39
       2786.38   6.973     46
       2783.69   6.966    399
       2781.86   6.961    128
       2776.86   6.949    116
       2774.90   6.944    392
       2772.22   6.937     49
       1608.64   4.026    246
       1602.17   4.009    525
       1595.58   3.993    261
       1049.07   2.625    164
       1041.38   2.606    212
       1033.57   2.587    181
        727.54   1.821     53
        721.07   1.805    137
        717.90   1.797     52
        714.60   1.789    139
        713.62   1.786    168
        712.04   1.782    116
        711.43   1.781    115
        708.13   1.772     63
        705.81   1.767    158
        699.34   1.750     70
        663.94   1.662     32
        656.37   1.643     87
        648.93   1.624    118
        645.87   1.617     70
        643.07   1.610     67
        641.36   1.605     95
        633.79   1.586     38
        619.14   1.550     36
        611.69   1.531    120
        605.96   1.517     71
        604.00   1.512    181
        598.51   1.498     76
        596.44   1.493    189
        591.19   1.480     36
        589.11   1.475    121
        581.79   1.456     36
        547.36   1.370     32
        540.65   1.353     80
        538.21   1.347    170
        534.42   1.338    259
        531.13   1.329    299
        527.22   1.320    183
        523.80   1.311     77
        522.34   1.307     78
        519.04   1.299     43
        400.15   1.002    483
        392.70   0.983   1000
        385.38   0.965    423
        364.87   0.913    213
        357.91   0.896    696
        354.00   0.886     80
        350.83   0.878    215
    

in CDCl3



KBr disc



nujol mull