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MS-NW-2894 1-chloromethoxy-2-methoxyethane C4H9ClO2 (Mass of molecular ion: 124)
Source Temperature: 210 °C Sample Temperature: 180 °C Reservoir, 75 eV
14.0 1.1 15.0 14.7 26.0 1.6 27.0 5.1 28.0 5.7 29.0 17.0 30.0 3.1 31.0 13.6 36.0 1.5 43.0 8.0 44.0 6.9 45.0 100.0 46.0 2.1 49.0 9.8 51.0 3.4 58.0 20.6 59.0 37.3 60.0 13.7 63.0 1.2 73.0 1.0 79.0 4.6 81.0 1.5 88.0 7.1 89.0 13.2 93.0 1.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C4 H9 Cl O2 0.05 ml : 0.5 ml CDCl3 1-chloromethoxy-2-methoxyethane Assign. Shift(ppm)
A 5.542 B 3.83 C 3.60 D 3.389
Hz ppm Int.
496.38 5.543 571 349.00 3.897 52 348.13 3.888 50 345.31 3.856 96 344.00 3.842 72 342.00 3.819 87 339.88 3.795 110 338.94 3.785 111 326.69 3.648 119 325.69 3.637 111 323.63 3.614 103 321.63 3.592 86 320.44 3.578 112 317.50 3.546 66 316.56 3.535 62 303.50 3.389 1000
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