-
MassMS-IW-3679 4-chloro-1,3-dioxolan-2-one C3H3ClO3 (Mass of molecular ion: 122)
Source Temperature: 210 °C Sample Temperature: 160 °C Reservoir, 75 eV
13.0 1.6 14.0 8.6 15.0 49.2 16.0 1.2 25.0 1.0 26.0 4.6 27.0 6.6 28.0 11.5 29.0 71.2 30.0 19.0 31.0 6.0 35.0 4.7 36.0 4.7 37.0 1.6 38.0 1.8 41.0 2.1 42.0 15.7 43.0 93.5 44.0 18.5 45.0 3.4 47.0 2.5 48.0 27.0 49.0 37.1 50.0 91.0 51.0 13.1 52.0 35.1 58.0 33.1 59.0 1.8 61.0 1.6 62.0 2.3 63.0 10.7 65.0 3.9 73.0 3.3 76.0 2.9 77.0 2.0 78.0 19.3 79.0 1.4 80.0 6.0 86.0 1.5 87.0 100.0 88.0 9.6 89.0 1.1 93.0 1.3 94.0 1.7 97.0 1.9 99.0 1.1 122.0 3.7 124.0 1.2 131.0 1.0
400 MHz in CDCl3
-
1H NMR 399.65 MHz C3 H3 Cl O3 0.05 ml : 0.5 ml CDCl3 4-chloro-1,3-dioxolan-2-one 
Assign. Shift(ppm)
A 6.504 B 4.893 C 4.642 J(B,C)=-10.2HZ J(B,A)=5.7HZ J(C,A)=2.0HZ
Hz ppm Int.2603.30 6.514 854 2601.32 6.509 911 2597.66 6.500 893 2595.67 6.495 945 1963.96 4.915 770 1958.31 4.901 779 1953.74 4.889 943 1948.09 4.875 927 1860.96 4.657 975 1859.13 4.652 1000 1853.64 4.639 33 1850.59 4.631 841 1848.75 4.626 887
in CDCl3
liquid film
更多供应商
