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2-氯-4-氨基苯酚

产品名称 2-氯-4-氨基苯酚

CAS号3964-52-1

分子式C6H6ClNO

分子量143.57


  • Mass

    MS-KW-0536          
    4-amino-2-chlorophenol
    C6H6ClNO            (Mass of molecular ion:    143)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       1.3
          26.0       1.3
          27.0       2.3
          28.0       5.7
          29.0       1.2
          37.0       1.1
          38.0       1.6
          38.5       3.5
          39.0       3.2
          39.5       7.7
          40.0       1.1
          41.0       1.3
          50.0       2.5
          51.0       9.5
          52.0      37.0
          53.0      13.7
          53.5       4.6
          54.0       3.3
          55.0       1.1
          61.0       1.8
          62.0       2.3
          63.0       3.2
          68.0       1.0
          71.5       6.9
          72.5       2.3
          73.0       1.2
          78.0       7.5
          79.0      68.4
          80.0      14.7
          81.0       2.4
          87.0       1.8
          89.0       1.1
          90.0       1.0
         106.0       1.5
         107.0       2.2
         108.0       1.4
         114.0       3.8
         115.0       1.6
         116.0       1.5
         142.0       6.9
         143.0     100.0
         144.0       9.4
         145.0      32.0
         146.0       2.3
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C6H6ClNO 0.039 g : 0.5 ml DMSO-d6
    4-amino-2-chlorophenol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.91 B 6.677 C 6.574 D 6.394 E 4.66

         Hz     ppm     Int.
    

       3563.39   8.914    309
       2673.80   6.689    870
       2665.26   6.667    994
       2629.40   6.578    980
       2626.81   6.571   1000
       2561.04   6.407    566
       2558.45   6.400    520
       2552.50   6.385    488
       2549.90   6.379    445
       1862.95   4.660    351
    

in DMSO-d6



KBr disk



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