3-硝基溴苄

产品名称 3-硝基溴苄

CAS号3958-57-4

分子式C7H6BrNO2

分子量216.03

¹³CNMR

Mass

MS-IW-0608          
3-nitrobenzyl bromide
C7H6BrNO2           (Mass of molecular ion:    215)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      39.0       1.8
      51.0       1.4
      62.0       1.2
      63.0       3.6
      64.0       1.4
      78.0       1.6
      89.0      10.4
      90.0      28.4
      91.0       2.3
     136.0     100.0
     137.0       8.2
     169.0       1.1
     171.0       1.1
     215.0       3.3
     217.0       3.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₆ Br N O₂	0.040 g : 0.5 ml CDCl₃
3-nitrobenzyl bromide

    Assign.     Shift(ppm)

      A             8.267
      B             8.168
      C             7.742
      D             7.551
      E             4.550

     Hz     ppm     Int.

   3305.91   8.273    187
   3304.20   8.268    284
   3302.49   8.264    188
   3269.17   8.181    136
   3268.07   8.178    126
   3260.99   8.160    144
   3259.77   8.157    132
   3098.27   7.753    149
   3090.58   7.734    176
   3025.27   7.570    165
   3017.33   7.550    258
   3013.43   7.541     23
   3009.28   7.530    127
   1818.60   4.551   1000

in CDCl3

KBr disc

nujol mull

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