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MS-KW-0279 4-bromo-2-chloroaniline C6H5BrClN (Mass of molecular ion: 205)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 2.5 36.0 1.0 37.0 3.4 38.0 4.4 39.0 3.9 40.0 1.2 41.0 3.6 44.5 6.5 45.0 2.7 45.5 5.1 49.0 1.6 50.0 2.2 51.0 1.3 52.0 7.0 61.0 4.5 62.0 7.7 62.5 7.3 63.0 22.8 63.5 2.5 64.0 6.8 65.0 3.5 72.0 1.0 73.0 4.2 74.0 2.4 75.0 2.5 84.5 1.2 85.5 1.2 88.0 1.2 89.0 2.1 90.0 42.2 91.0 9.3 97.0 1.3 98.0 1.1 99.0 12.2 100.0 1.3 101.0 4.0 102.5 5.8 103.5 7.5 104.5 1.8 125.0 2.5 126.0 25.5 127.0 2.9 128.0 8.2 143.0 1.4 145.0 1.2 169.0 1.3 170.0 1.0 171.0 1.3 177.0 1.9 179.0 2.5 205.0 77.0 206.0 6.3 207.0 100.0 208.0 7.3 209.0 24.1 210.0 1.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H5 Br Cl N 0.035 g : 0.5 ml CDCl3 4-bromo-2-chloroaniline Assign. Shift(ppm)
A 7.370 B 7.149 C 6.628 D 4.05
Hz ppm Int.
2946.78 7.374 840 2944.58 7.368 874 2862.67 7.163 478 2860.47 7.158 452 2854.13 7.142 516 2851.93 7.137 489 2652.83 6.638 1000 2644.29 6.617 929 1617.19 4.047 190
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