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MS-IW-9001 1-bromo-2,3-difluorobenzene C6H3BrF2 (Mass of molecular ion: 192)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
31.0 5.6 37.0 4.4 38.0 1.5 49.0 1.1 50.0 4.0 56.0 3.6 57.0 2.6 61.0 5.2 62.0 10.6 63.0 42.0 64.0 2.3 68.0 7.0 69.0 2.6 73.0 1.1 74.0 4.6 75.0 2.1 79.0 1.5 80.0 1.6 81.0 4.2 87.0 3.0 92.0 2.5 93.0 6.6 94.0 3.2 96.0 3.3 97.0 3.2 111.0 1.0 112.0 7.6 113.0 84.9 114.0 5.7 192.0 100.0 193.0 7.2 194.0 98.9 195.0 6.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H3 Br F2 0.05 ml : 0.5 ml CDCl3 1-bromo-2,3-difluorobenzene Assign. Shift(ppm)
A 7.296 B 7.111 C 6.976
Hz ppm Int.
2924.93 7.319 551 2923.22 7.315 847 2921.51 7.311 569 2919.19 7.305 587 2917.48 7.301 971 2916.75 7.299 779 2915.77 7.296 774 2915.04 7.294 1000 2913.33 7.290 642 2911.01 7.284 619 2909.30 7.280 945 2907.59 7.276 604 2855.96 7.147 478 2854.37 7.143 471 2848.88 7.129 540 2847.41 7.125 966 2846.07 7.122 927 2844.60 7.118 524 2840.45 7.108 712 2838.99 7.104 919 2837.65 7.101 956 2836.18 7.097 639 2830.69 7.083 651 2829.10 7.079 599 2799.07 7.004 665 2797.12 6.999 656 2793.95 6.991 691 2791.99 6.987 727 2790.77 6.984 926 2788.94 6.979 910 2785.77 6.971 887 2783.81 6.966 929 2782.47 6.963 515 2780.52 6.958 467 2777.34 6.950 448 2775.39 6.945 435
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