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MassMS-IW-7441 2-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluorononyl)oxirane C11H5F17O (Mass of molecular ion: 476)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 4.8 27.0 8.1 28.0 4.4 29.0 36.2 30.0 1.4 31.0 26.3 33.0 2.3 39.0 2.4 41.0 4.8 42.0 2.3 43.0 45.3 44.0 1.9 47.0 2.8 51.0 17.5 55.0 1.8 57.0 91.7 58.0 3.9 59.0 19.9 61.0 2.6 64.0 1.8 65.0 4.7 69.0 45.7 71.0 2.0 75.0 2.4 76.0 1.5 77.0 21.0 78.0 1.2 79.0 7.0 81.0 1.0 87.0 1.3 88.0 1.3 89.0 3.3 90.0 1.1 91.0 5.5 93.0 1.6 95.0 8.7 100.0 7.0 101.0 1.2 105.0 1.0 107.0 100.0 108.0 6.0 109.0 15.4 113.0 1.8 115.0 1.2 119.0 15.6 120.0 1.1 121.0 1.0 122.0 1.1 127.0 2.4 131.0 14.9 133.0 1.2 139.0 2.9 145.0 1.5 157.0 1.1 169.0 7.3 170.0 1.4 181.0 2.9 231.0 1.8 339.0 1.6 345.0 1.6 363.0 1.4 389.0 1.8 428.0 1.1 437.0 1.2 441.0 3.3 461.0 2.3 476.0 22.0 477.0 2.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H5 F17 O 0.05 ml : 0.5 ml CDCl3 2-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,9-heptadecafluorononyl)oxirane 
Assign. Shift(ppm)
A 3.223 B 2.878 C 2.582 D *1 2.416 E *1 2.254
Hz ppm Int.1297.24 3.246 148 1294.80 3.240 185 1293.46 3.237 219 1291.26 3.231 391 1288.70 3.225 373 1288.09 3.224 386 1285.52 3.217 403 1283.45 3.212 236 1282.10 3.209 218 1279.54 3.202 176 1154.79 2.890 656 1154.42 2.889 666 1150.27 2.879 1000 1146.12 2.868 701 1145.63 2.867 680 1035.77 2.592 784 1033.33 2.586 808 1031.01 2.580 770 1028.44 2.574 739 995.97 2.493 58 989.99 2.478 55 978.52 2.449 158 976.68 2.444 121 972.53 2.434 150 963.01 2.410 191 957.03 2.395 192 945.19 2.366 102 939.21 2.351 95 928.10 2.323 99 922.73 2.309 96 909.79 2.277 212 908.08 2.273 169 904.42 2.264 195 894.65 2.239 145 892.94 2.235 142 891.60 2.231 153 889.53 2.226 175 887.70 2.222 137 886.47 2.219 129 876.46 2.194 70 875.00 2.190 46 871.09 2.180 66 869.63 2.176 42
liquid film
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