-
MassMS-IW-9290 4-pyridineethanol hydrochloride C7H9NO HCl (Mass of molecular ion: 123)
Source Temperature: 170 °C Sample Temperature: 130 °C Direct, 75 eV
26.0 1.6 27.0 2.6 28.0 4.2 29.0 1.7 31.0 22.4 35.0 3.5 36.0 29.4 37.0 2.1 38.0 11.6 39.0 18.0 40.0 3.7 41.0 3.4 43.0 1.2 50.0 4.0 51.0 8.7 52.0 5.9 53.0 2.2 54.0 3.9 62.0 1.1 63.0 3.5 64.0 2.3 65.0 16.3 66.0 13.7 67.0 7.1 77.0 1.9 78.0 3.5 79.0 1.5 80.0 1.3 92.0 19.2 93.0 100.0 94.0 8.2 104.0 1.3 105.0 2.0 106.0 1.0 123.0 51.6 124.0 4.6
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C7 H9 N O 0.034 g : 0.5 ml DMSO-d6 4-pyridineethanol hydrochloride 
Assign. Shift(ppm)
A 8.861 B 8.002 C 3.766 D 3.052
Hz ppm Int.3545.17 8.871 762 3538.57 8.855 802 3201.29 8.011 750 3194.58 7.994 721 1511.47 3.782 517 1508.54 3.775 136 1505.37 3.767 1000 1501.95 3.759 131 1499.27 3.752 550 1226.44 3.069 433 1220.34 3.054 786 1214.36 3.039 389
in DMSO-d6
KBr disc
nujol mull
更多供应商