(-)-顺-6,6-二甲基双环[3.1.1]-2-氨甲基

Mass

MS-NW-7473          
(-)-cis-myrtanylamine
C10H19N             (Mass of molecular ion:    153)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      27.0       2.7
      28.0       1.7
      29.0       1.9
      30.0     100.0
      31.0       1.7
      39.0       3.9
      41.0       9.7
      42.0       1.3
      43.0       3.6
      53.0       2.5
      54.0       3.2
      55.0       3.6
      56.0       4.0
      57.0       1.0
      58.0       1.5
      65.0       1.0
      67.0       8.3
      68.0       2.5
      69.0       6.8
      70.0       2.6
      71.0       5.5
      77.0       1.8
      79.0       3.9
      80.0       1.7
      81.0       6.0
      82.0       4.3
      83.0       1.1
      84.0       2.1
      91.0       1.4
      93.0       4.0
      94.0       1.3
      95.0       1.5
      96.0       1.2
     107.0       1.5
     110.0       3.1
     121.0       1.6
     123.0       1.3
     124.0       1.2
     136.0       1.0
     138.0       3.7

Assign. Shift(ppm) A 2.66 B 2.359 C 2.00 to 1.88 D 1.61 E 1.443 F 1.185 G 0.973 J 0.905

     Hz     ppm     Int.

   1068.85   2.675    138
   1061.89   2.658    212
   1054.93   2.640    121
    949.22   2.376     59
    947.39   2.371     54
    946.41   2.369     61
    943.24   2.361     57
    941.16   2.355     52
    939.82   2.352     65
    937.99   2.348     55
    809.20   2.025     56
    807.50   2.021     59
    802.25   2.008     58
    800.78   2.004     70
    799.80   2.002     73
    796.39   1.993     70
    793.46   1.986     86
    791.63   1.981     73
    788.45   1.973    130
    787.11   1.970    174
    785.28   1.965    111
    781.98   1.957    105
    779.30   1.950    117
    777.10   1.945    124
    775.39   1.941    113
    774.41   1.938    109
    771.97   1.932     84
    766.72   1.919    135
    765.38   1.916    143
    763.31   1.910    176
    760.50   1.903    139
    757.93   1.897    125
    755.37   1.891     83
    753.78   1.887     87
    752.56   1.884     83
    749.27   1.875     51
    747.19   1.870     67
    744.63   1.864     53
    741.46   1.856     55
    643.92   1.612     75
    588.75   1.474     49
    582.40   1.458     60
    578.00   1.447     51
    574.46   1.438     58
    473.88   1.186   1000
    388.92   0.974    987
    366.58   0.918    206
    357.06   0.894    200