400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H15 N O8 0.040 g : 0.5 ml DMSO-d6 p-nitrophenyl alpha-D-glucopyranoside 
Assign. Shift(ppm)
A 8.230 B 7.301 C 5.649 D 5.26 E 5.09 F 5.07 G 4.54 J 3.658 K *1 3.571 L *1 3.48 M 3.441 N 3.393 D 3.233 THE H2O SIGNAL ABOUT 3.45 PPM REMOVED. ASSIGNED BY H-H COSY AND ADDITION OF D2O. J(C,M) = 3.4 HZ J(D,M) = 6.1 HZ J(E,P) = 5.7 HZ J(F,J) = 5.1 HZ J(G,K) = 5.6 HZ J(G,L) = 5.9 HZ J(J,M) = 9.5 HZ J(J,P) = 8.9 HZ J(K,L) = -11.7 HZ J(K,N) = 2.0 HZ J(L,N) = 5.3 HZ J(N,P) = 10.1 HZ
Hz ppm Int.3297.49 8.251 76 3294.07 8.243 895 3291.75 8.237 262 3289.31 8.231 45 3286.87 8.225 252 3284.67 8.219 1000 3281.25 8.211 101 2926.03 7.322 84 2922.61 7.313 881 2920.29 7.308 256 2917.85 7.302 47 2915.53 7.296 238 2913.21 7.290 857 2909.79 7.281 91 2259.52 5.654 370 2255.98 5.645 377 2107.18 5.273 520 2100.95 5.257 536 2036.13 5.095 509 2030.03 5.080 805 2024.78 5.067 523 1819.82 4.554 183 1814.09 4.540 450 1808.23 4.525 192 1474.73 3.691 81 1469.73 3.678 84 1465.33 3.667 142 1460.33 3.655 148 1456.42 3.645 118 1451.29 3.632 124 1438.72 3.600 64 1436.52 3.595 73 1432.86 3.586 69 1430.79 3.581 85 1426.76 3.571 132 1424.68 3.565 123 1422.85 3.561 64 1421.02 3.556 124 1419.07 3.551 116 1403.08 3.511 90 1397.46 3.497 176 1391.48 3.482 181 1389.89 3.478 184 1385.99 3.469 222 1383.67 3.463 167 1380.00 3.454 305 1376.46 3.445 194 1373.05 3.436 375 1370.48 3.430 270 1364.01 3.414 151 1362.06 3.409 125 1358.64 3.400 99 1356.57 3.395 83 1353.88 3.388 129 1351.93 3.383 136 1348.88 3.376 116 1346.68 3.370 96 1303.71 3.263 118 1297.97 3.248 119 1294.92 3.241 136 1293.95 3.238 121 1291.63 3.232 34 1289.18 3.226 134 1288.21 3.224 125 1285.16 3.216 88 1279.30 3.202 83
in DMSO-d6
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