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MS-IW-9525 2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoro-1-heptanol C7H3F13O (Mass of molecular ion: 350)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
29.0 10.0 30.0 1.1 31.0 100.0 32.0 1.2 33.0 3.1 43.0 1.0 49.0 8.0 51.0 4.0 61.0 5.2 69.0 13.2 81.0 2.7 93.0 1.0 95.0 1.0 100.0 3.4 113.0 1.7 119.0 3.1 131.0 8.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7H3F13O 0.05 ml : 0.5 ml DMSO-d6 2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoro-1-heptanol Assign. Shift(ppm)
A 6.13 B 3.988
Hz ppm Int.
2449.47 6.127 484 2442.88 6.111 1000 2436.16 6.094 491 1614.87 4.040 234 1608.28 4.023 232 1599.74 4.002 467 1593.14 3.986 440 1584.72 3.964 244 1578.01 3.948 225
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