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MassMS-NW-1087 3-(aminomethyl)pyridine C6H8N2 (Mass of molecular ion: 108)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
18.0 1.5 26.0 1.4 27.0 3.0 28.0 12.1 29.0 2.7 30.0 25.6 37.0 1.0 38.0 2.2 39.0 6.5 40.0 1.2 41.0 1.4 50.0 4.0 51.0 7.4 52.0 8.9 53.0 7.4 54.0 2.7 63.0 2.8 64.0 3.3 65.0 6.1 78.0 4.2 79.0 15.5 80.0 100.0 81.0 6.1 91.0 3.1 92.0 4.4 105.0 1.5 107.0 22.4 108.0 9.6
90 MHz in CDCl3
parameter in DMSO-d6
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1H NMR 89.56 MHz C6 H8 N2 0.04 ml : 0.5 ml CDCl3 3-(aminomethyl)pyridine 
Assign. Shift(ppm)
A 8.52 B 7.663 C 7.262 D 3.893 E 1.54
Hz ppm Int.768.06 8.576 156 767.31 8.568 165 766.50 8.559 144 765.75 8.551 178 765.00 8.542 174 764.19 8.533 155 763.81 8.529 148 762.00 8.509 141 758.94 8.475 130 757.25 8.456 133 692.75 7.736 67 691.00 7.716 95 690.44 7.710 94 684.94 7.648 101 684.25 7.641 74 683.94 7.637 76 683.25 7.629 138 682.63 7.623 136 682.00 7.616 72 680.94 7.604 90 656.19 7.327 132 655.25 7.317 128 651.38 7.274 123 650.50 7.264 117 648.38 7.240 91 647.44 7.230 87 643.56 7.186 82 642.69 7.177 76 348.69 3.894 776 138.31 1.545 1000
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1H NMR 300 MHz C6 H8 N2 30 % in DMSO 3-(aminomethyl)pyridine Parameter ppm Hz
D(A) 8.75 D(B) 7.88 D(C) 7.42 D(D) 8.59 D(E) 3.85 J(A,B) 2.0 J(A,C) 0.7 J(A,D) 0.3 J(A,E) 0.0 J(B,C) 7.8 J(B,D) 1.7 J(B,E) 0.7 J(C,D) 4.9 J(C,E) 0.0 J(D,E) 0.0 D(F) 2.06 BRUEGEL,W. Z.ELEKTROCHEM.(BER.BUNSENGES.PHYS.CHEM.) 66, 159 (1962) J(A,D) LESS THAN 0.3HZ.
Hz ppm Int.2625.85 8.753 182 2624.12 8.747 192 2580.34 8.601 125 2578.66 8.596 128 2575.44 8.585 130 2573.76 8.579 130 2369.81 7.899 52 2368.07 7.894 87 2366.27 7.888 53 2361.99 7.873 61 2360.26 7.868 96 2358.46 7.862 57 2232.45 7.441 95 2232.08 7.440 95 2227.55 7.425 96 2227.12 7.424 96 2224.70 7.416 89 2224.27 7.414 88 2219.80 7.399 83 2219.37 7.398 83 1155.31 3.851 671 1154.75 3.849 671 617.98 2.060 1000
in CDCl3
CCl4 solution
liquid film
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