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3-氨甲基吡啶

产品名称 3-氨甲基吡啶

CAS号3731-52-0

分子式C6H8N2

分子量108.14

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  • Mass

    MS-NW-1087          
    3-(aminomethyl)pyridine
    C6H8N2              (Mass of molecular ion:    108)
    

       Source Temperature: 250 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          18.0       1.5
          26.0       1.4
          27.0       3.0
          28.0      12.1
          29.0       2.7
          30.0      25.6
          37.0       1.0
          38.0       2.2
          39.0       6.5
          40.0       1.2
          41.0       1.4
          50.0       4.0
          51.0       7.4
          52.0       8.9
          53.0       7.4
          54.0       2.7
          63.0       2.8
          64.0       3.3
          65.0       6.1
          78.0       4.2
          79.0      15.5
          80.0     100.0
          81.0       6.1
          91.0       3.1
          92.0       4.4
         105.0       1.5
         107.0      22.4
         108.0       9.6
    

90 MHz in CDCl3

parameter in DMSO-d6


  • 1H NMR 89.56 MHz
    C6 H8 N2 0.04 ml : 0.5 ml CDCl3
    3-(aminomethyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.52 B 7.663 C 7.262 D 3.893 E 1.54

         Hz     ppm     Int.
    

        768.06   8.576    156
        767.31   8.568    165
        766.50   8.559    144
        765.75   8.551    178
        765.00   8.542    174
        764.19   8.533    155
        763.81   8.529    148
        762.00   8.509    141
        758.94   8.475    130
        757.25   8.456    133
        692.75   7.736     67
        691.00   7.716     95
        690.44   7.710     94
        684.94   7.648    101
        684.25   7.641     74
        683.94   7.637     76
        683.25   7.629    138
        682.63   7.623    136
        682.00   7.616     72
        680.94   7.604     90
        656.19   7.327    132
        655.25   7.317    128
        651.38   7.274    123
        650.50   7.264    117
        648.38   7.240     91
        647.44   7.230     87
        643.56   7.186     82
        642.69   7.177     76
        348.69   3.894    776
        138.31   1.545   1000
    


  • 1H NMR 300 MHz
    C6 H8 N2 30 % in DMSO
    3-(aminomethyl)pyridine
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 8.75 D(B) 7.88 D(C) 7.42 D(D) 8.59 D(E) 3.85 J(A,B) 2.0 J(A,C) 0.7 J(A,D) 0.3 J(A,E) 0.0 J(B,C) 7.8 J(B,D) 1.7 J(B,E) 0.7 J(C,D) 4.9 J(C,E) 0.0 J(D,E) 0.0 D(F) 2.06 BRUEGEL,W. Z.ELEKTROCHEM.(BER.BUNSENGES.PHYS.CHEM.) 66, 159 (1962) J(A,D) LESS THAN 0.3HZ.

         Hz     ppm     Int.
    

       2625.85   8.753    182
       2624.12   8.747    192
       2580.34   8.601    125
       2578.66   8.596    128
       2575.44   8.585    130
       2573.76   8.579    130
       2369.81   7.899     52
       2368.07   7.894     87
       2366.27   7.888     53
       2361.99   7.873     61
       2360.26   7.868     96
       2358.46   7.862     57
       2232.45   7.441     95
       2232.08   7.440     95
       2227.55   7.425     96
       2227.12   7.424     96
       2224.70   7.416     89
       2224.27   7.414     88
       2219.80   7.399     83
       2219.37   7.398     83
       1155.31   3.851    671
       1154.75   3.849    671
        617.98   2.060   1000
    

in CDCl3



CCl4 solution



liquid film