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MassMS-NW-5719 2-(aminomethyl)pyridine C6H8N2 (Mass of molecular ion: 108)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 3.4 26.0 3.1 27.0 7.4 28.0 14.6 29.0 2.6 30.0 57.9 31.0 1.0 37.0 1.8 38.0 3.1 39.0 7.6 40.0 1.4 41.0 1.7 49.0 1.6 50.0 8.0 51.0 15.1 52.0 29.3 53.0 17.4 54.0 2.5 62.0 1.2 63.0 2.4 64.0 1.9 65.0 4.5 66.0 1.0 75.0 1.2 76.0 1.7 77.0 1.9 78.0 12.5 79.0 70.2 80.0 100.0 81.0 6.1 92.0 2.3 93.0 3.3 104.0 3.6 105.0 4.8 107.0 49.1 108.0 83.3 109.0 6.3 195.0 1.1
parameter in DMSO-d6
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1H NMR 300 MHz C6 H8 N2 30 % in DMSO 2-(aminomethyl)pyridine 
Parameter ppm Hz
D(A) 8.64 D(B) 7.29 D(C) 7.82 D(D) 7.58 D(E) 3.94 J(A,B) 5.0 J(A,C) 2.1 J(A,D) 0.8 J(A,E) 0.0 J(B,C) 7.7 J(B,D) 1.2 J(B,E) 0.5 J(C,D) 8.0 J(C,E) 0.0 J(D,E) 0.5 D(F) 2.08 BRUEGEL,W. Z.ELEKTROCHEM.BER.BUNSENGES.PHYS.CHEM. 66, 159 (1962)
Hz ppm Int.2595.89 8.653 88 2595.22 8.651 93 2593.89 8.646 96 2593.22 8.644 94 2590.91 8.636 94 2590.24 8.634 97 2588.90 8.630 95 2588.17 8.627 89 2355.22 7.851 57 2353.16 7.844 57 2347.38 7.825 123 2345.31 7.818 118 2339.54 7.798 79 2337.47 7.792 77 2277.96 7.593 130 2269.75 7.566 107 2193.27 7.311 66 2187.68 7.292 71 2186.16 7.287 68 2181.06 7.270 59 2180.63 7.269 59 1182.08 3.940 758 624.02 2.080 1000
in CDCl3
liquid film
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