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4,4'-二甲氨基二苯酮

产品名称 4,4'-二甲氨基二苯酮

CAS号3708-39-2

分子式C15H16N2O

分子量240.3

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  • Mass

    MS-IW-2159          
    4,4'-bis(methylamino)benzophenone
    C15H16N2O           (Mass of molecular ion:    240)
    

       Source Temperature: 130 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          28.0       1.5
          39.0       1.3
          50.0       1.0
          51.0       1.3
          63.0       1.2
          64.0       1.3
          65.0       5.1
          76.0       2.0
          77.0       9.0
          78.0       2.9
          79.0       6.3
          91.0       1.8
         104.0       2.3
         105.0       8.1
         105.5       4.4
         106.0      21.7
         106.5       1.9
         107.0       1.6
         119.0       1.7
         120.0       1.9
         132.0       1.6
         134.0     100.0
         135.0       9.3
         197.0       1.1
         209.0       1.3
         210.0      14.1
         211.0       7.5
         212.0       2.0
         223.0       9.6
         224.0       2.5
         225.0       1.4
         226.0       1.2
         239.0      24.4
         240.0      89.7
         241.0      15.2
         242.0       1.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15 H16 N2 O 0.056 g : 0.5 ml CDCl3
    4,4'-bis(methylamino)benzophenone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.691 B 6.551 C 4.42 D 2.834 J(C,D)=5.2HZ

         Hz     ppm     Int.
    

       3081.05   7.710    102
       3078.49   7.703    810
       3076.42   7.698    271
       3074.22   7.693     55
       3071.66   7.686    261
       3069.58   7.681    843
       3067.02   7.675    132
       2625.49   6.570    107
       2622.92   6.564    806
       2620.85   6.558    265
       2616.09   6.546    246
       2614.14   6.542    772
       2611.45   6.535    120
       1766.97   4.422    123
       1762.08   4.410    125
       1135.38   2.841   1000
       1130.25   2.829    971
    

in CDCl3



KBr disc



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