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网站主页CAS数据库列表 3634-67-1更多图谱氯三己基硅烷(3634-67-1)质谱(MS)

氯三己基硅烷

产品名称 氯三己基硅烷

CAS号3634-67-1

分子式C18H39ClSi

分子量319.04


  • Mass

    MS-NW-7618          
    chlorotrihexylsilane
    C18H39ClSi          (Mass of molecular ion:    318)
    

       Source Temperature: 250 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          27.0       3.5
          28.0       1.9
          29.0       5.9
          39.0       1.8
          41.0       8.7
          42.0       2.0
          43.0       9.3
          55.0       6.5
          56.0       2.0
          57.0       1.6
          59.0       1.3
          63.0       5.8
          65.0       5.6
          67.0       1.4
          69.0       3.4
          71.0       1.1
          78.0       1.8
          79.0      11.2
          80.0       1.3
          81.0       4.2
          83.0       8.7
          84.0       1.3
          85.0       2.2
          91.0       5.0
          92.0       2.8
          93.0      21.5
          94.0       2.4
          95.0       7.3
          97.0       3.2
         105.0       4.5
         106.0       1.6
         107.0      29.6
         108.0       2.9
         109.0      10.6
         111.0       1.4
         113.0       1.9
         117.0       1.5
         119.0      10.8
         120.0       2.5
         121.0       8.2
         122.0       1.4
         123.0       1.8
         131.0       1.8
         133.0       3.5
         134.0       1.1
         135.0       1.6
         147.0       4.3
         148.0       1.2
         149.0      74.7
         150.0       9.2
         151.0      26.9
         152.0       3.2
         153.0       1.0
         163.0       2.0
         177.0       1.6
         191.0       1.2
         199.0       1.3
         205.0       1.0
         215.0       1.6
         217.0       1.3
         233.0     100.0
         234.0      18.7
         235.0      37.3
         236.0       6.7
         237.0       1.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C18 H39 Cl Si 0.05 ml : 0.5 ml CDCl3
    chlorotrihexylsilane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 1.34 B 1.29 C 0.887 D 0.792

         Hz     ppm     Int.
    

        571.29   1.430     38
        568.60   1.423     45
        562.74   1.409     96
        561.28   1.405     94
        556.40   1.393    154
        555.30   1.390    149
        554.20   1.387    148
        547.36   1.370    195
        544.92   1.364    215
        543.58   1.361    230
        540.65   1.353    264
        534.18   1.337    228
        532.59   1.333    212
        529.91   1.326    224
        525.39   1.315    262
        524.05   1.312    279
        522.22   1.307    266
        517.82   1.296    399
        515.26   1.290    582
        512.94   1.284    481
        508.91   1.274    383
        361.69   0.906    349
        354.86   0.888   1000
        347.90   0.871    436
        334.23   0.837     34
        325.44   0.815    283
        318.12   0.796    217
        315.80   0.791    171
        314.58   0.788    155
        309.33   0.775    313
    

in CDCl3



liquid film