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MS-IW-0067 (dimethylamino)acetaldehyde diethyl acetal C8H19NO2 (Mass of molecular ion: 161)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.6 27.0 2.4 28.0 1.9 29.0 6.3 30.0 4.2 31.0 1.3 42.0 6.7 43.0 4.0 44.0 8.2 45.0 4.3 47.0 38.9 56.0 1.4 57.0 2.0 58.0 100.0 59.0 5.1 70.0 1.5 71.0 1.5 72.0 29.6 73.0 4.4 75.0 32.5 76.0 1.1 79.0 1.3 86.0 3.0 88.0 4.7 103.0 43.0 104.0 2.5 116.0 31.4 117.0 15.1 118.0 1.0 161.0 2.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H19 N O2 0.05 ml : 0.5 ml CDCl3 (dimethylamino)acetaldehyde diethyl acetal Assign. Shift(ppm)
A 4.608 B 3.617 C 2.469 D 2.292 E 1.222
Hz ppm Int.
418.19 4.670 40 412.88 4.611 83 407.63 4.552 43 336.75 3.761 39 331.75 3.705 68 329.56 3.680 106 324.69 3.626 118 322.44 3.601 118 317.69 3.548 109 315.38 3.522 68 310.81 3.471 43 223.75 2.499 152 218.44 2.440 144 205.31 2.293 1000 116.25 1.299 280 114.00 1.273 30 109.25 1.220 598 102.19 1.142 237
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