双巯乙基硫醚

Mass

MS-IW-6260          
2,2'-thiodiethanethiol
C4H10S3             (Mass of molecular ion:    154)

   Source Temperature: 200 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      26.0       1.2
      27.0       8.9
      28.0       2.7
      32.0       1.4
      33.0       1.5
      34.0       4.0
      35.0       8.0
      44.0       1.3
      45.0      14.2
      46.0       4.4
      47.0      10.2
      57.0       1.6
      58.0       6.1
      59.0      19.5
      60.0      31.7
      61.0     100.0
      62.0       5.3
      63.0       6.0
      64.0       2.6
      65.0       1.6
      73.0       1.1
      78.0       1.3
      79.0       1.5
      87.0       1.7
      91.0       1.0
      92.0       2.3
      93.0       2.4
      94.0      55.1
      95.0       3.7
      96.0       5.0
      97.0       1.1
     105.0       2.0
     106.0       1.6
     107.0      11.2
     109.0       1.0
     120.0      21.6
     121.0       1.9
     122.0       2.0
     152.0       2.0
     154.0      24.1
     155.0       1.8
     156.0       3.2

Assign. Shift(ppm) A 2.78 B 2.73 C 1.711 CONFIRMED BY C-H COSY

     Hz     ppm     Int.

   1122.31   2.809    229
   1121.83   2.808    274
   1119.38   2.801    374
   1117.31   2.796    251
   1115.60   2.792    353
   1113.65   2.787    818
   1110.96   2.780    851
   1107.54   2.772    846
   1106.93   2.770    914
   1106.32   2.769    966
   1105.59   2.767    838
   1101.32   2.756    803
   1100.22   2.753    697
   1096.80   2.745    564
   1095.09   2.741    498
   1094.12   2.738    962
   1092.77   2.735    673
   1090.33   2.729    269
   1088.62   2.724    677
   1086.55   2.719    480
   1086.06   2.718    557
   1085.21   2.716    308
   1084.11   2.713    346
   1080.32   2.704    297
   1078.00   2.698    252
    715.21   1.790    556
    712.89   1.784     52
    707.40   1.771   1000
    700.68   1.754    243
    699.95   1.752    298
    699.34   1.750    433
    696.53   1.743     41