400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C15 H14 N2 O 0.029 g : 0.5 ml CDCl3 10,11-dihydro-5H-dibenz(b,f)azepine-5-carboxamide Assign. Shift(ppm)
A 7.387 B 7.20 C 7.19 D 5.09 E *1 3.41 F *1 2.82
Hz ppm Int.
2959.84 7.407 47 2957.28 7.400 142 2954.35 7.393 164 2953.25 7.390 130 2951.29 7.385 133 2949.46 7.381 147 2947.63 7.376 171 2945.43 7.371 57 2890.87 7.234 25 2888.67 7.229 41 2883.67 7.216 135 2878.66 7.203 458 2876.95 7.199 664 2874.27 7.192 1000 2865.23 7.170 23 2035.89 5.095 40 1361.69 3.408 46 1125.00 2.815 46
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1H NMR 89.56 MHz C15 H14 N2 O 0.021 g : 0.5 ml CDCl3 10,11-dihydro-5H-dibenz(b,f)azepine-5-carboxamide Assign. Shift(ppm)
A 7.37 B 7.25 to 7.11 C 4.99 D *1 3.29 E *1 2.89 400MHZ. : HSP-41-757
Hz ppm Int.
669.44 7.475 27 667.31 7.451 73 663.44 7.408 115 661.00 7.381 148 659.81 7.368 162 657.44 7.341 222 655.19 7.316 135 651.25 7.272 117 648.94 7.246 232 645.31 7.206 1000 642.38 7.173 715 636.50 7.107 88 633.69 7.076 38 633.25 7.071 36 447.38 4.996 114 295.13 3.296 57 259.44 2.897 60
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