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网站主页CAS数据库列表 3562-73-0更多图谱1-(4-联联苯基)乙醇(3562-73-0)核磁图(13CNMR)

1-(4-联联苯基)乙醇

产品名称 1-(4-联联苯基)乙醇

CAS号3562-73-0

分子式C14H14O

分子量198.26

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  • Mass

    MS2016-05336CW      
    1-(4-biphenylyl)ethanol
    C14H14O             (Mass of molecular ion:    198)
    

       Source Temperature: 240 °C
       Sample Temperature:  20 °C
       Direct, 70 eV
    

          43.0       8.4
          51.0       3.0
          63.0       2.2
          75.0       1.7
          76.0       6.4
          77.0      13.9
          78.0       1.7
          88.0       1.2
          89.0       2.7
          91.0       1.1
          91.5       8.5
          99.0       2.3
         102.0       1.8
         115.0       5.2
         121.0       1.6
         126.0       2.1
         127.0       4.6
         128.0       4.1
         129.0       3.6
         139.0       1.5
         150.0       2.0
         151.0       6.4
         152.0      23.1
         153.0      17.8
         154.0      15.3
         155.0      95.6
         156.0      12.4
         165.0       7.6
         166.0       2.6
         167.0       2.1
         176.0       1.7
         177.0       1.3
         178.0       8.2
         179.0       6.5
         180.0      21.6
         181.0      12.7
         182.0       3.0
         183.0     100.0
         184.0      13.8
         185.0       1.1
         196.0       2.6
         197.0       3.8
         198.0      63.5
         199.0       9.6
    

400 MHz in CDCl3

in DMSO-d6


  • 1H NMR 399.65 MHz
    C14 H14 O 0.039 g : 0.5 ml CDCl3
    1-(4-biphenylyl)ethanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.57 B 7.56 C 7.42 D 7.41 E 7.331 F 4.904 G 2.12 J 1.506

         Hz     ppm     Int.
    

       3029.42   7.581    230
       3028.08   7.577    313
       3026.12   7.572    133
       3024.41   7.568    365
       3022.34   7.563    270
       3021.00   7.560    357
       3019.78   7.557    321
       3017.94   7.552    199
       3015.99   7.547    505
       3014.04   7.542     96
       2973.75   7.441     53
       2972.90   7.439    121
       2972.05   7.437    190
       2970.21   7.433     83
       2968.38   7.428     91
       2966.55   7.423    486
       2964.84   7.419    494
       2963.50   7.416    215
       2959.96   7.407    133
       2958.50   7.403    425
       2957.03   7.400    272
       2955.08   7.395     64
       2936.77   7.349     83
       2935.55   7.346    153
       2934.20   7.342     89
       2930.18   7.332     64
       2928.10   7.327    174
       2926.03   7.322     52
       2922.12   7.312     42
       2920.78   7.309     72
       2919.56   7.306     39
       1969.60   4.929     40
       1963.13   4.913    121
       1956.79   4.897    124
       1950.32   4.881     43
        847.29   2.121    116
        605.35   1.515    980
        598.88   1.499   1000
        595.21   1.490     30
    



in DMSO-d6

in CDCl3





KBr disc



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