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MS-NW-6701 1-(o-methoxyphenyl)piperazine C11H16N2O (Mass of molecular ion: 192)
Source Temperature: 100 °C Sample Temperature: 90 °C Reservoir, 75 eV
15.0 1.6 18.0 1.1 27.0 2.4 28.0 7.8 29.0 5.5 30.0 4.3 39.0 2.9 41.0 1.5 42.0 3.4 51.0 2.8 52.0 1.4 56.0 10.8 57.0 5.4 63.0 1.4 64.0 1.3 65.0 5.3 77.0 4.1 78.0 2.0 79.0 1.8 91.0 2.9 92.0 2.4 93.0 1.9 104.0 1.2 106.0 2.2 107.0 1.5 120.0 9.6 121.0 4.9 122.0 1.2 134.0 8.0 135.0 11.9 136.0 4.9 137.0 2.0 150.0 100.0 151.0 10.0 191.0 1.2 192.0 50.9 193.0 7.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C11 H16 N2 O 0.038 g : 0.5 ml CDCl3 1-(o-methoxyphenyl)piperazine Assign. Shift(ppm)
A 6.99 to 6.85 B 3.853 C 3.04 D 1.81
Hz ppm Int.
625.75 6.987 34 622.50 6.951 103 621.25 6.937 275 620.69 6.931 300 618.69 6.909 116 617.56 6.896 137 615.63 6.874 46 615.19 6.870 48 613.81 6.854 27 612.63 6.841 24 345.13 3.854 759 277.94 3.104 24 276.81 3.091 29 276.13 3.084 32 272.00 3.038 1000 162.56 1.816 134
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