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网站主页CAS数据库列表 3535-83-9更多图谱四正庚基碘化铵(3535-83-9)核磁图(1HNMR)

四正庚基碘化铵

产品名称 四正庚基碘化铵

CAS号3535-83-9

分子式C28H60IN

分子量537.69

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  • Mass

    MS-IW-4181          
    tetraheptylammonium iodide
    C28H60IN            (Mass of molecular ion:    537)
    

       Source Temperature: 160 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          17.0       1.5
          18.0       8.5
          27.0       1.5
          29.0       3.6
          30.0       1.2
          39.0       1.0
          41.0       8.1
          42.0       2.3
          43.0      10.1
          44.0       3.4
          55.0       5.1
          56.0       1.9
          57.0      27.2
          58.0       5.4
          69.0       1.0
          70.0       1.6
          71.0       1.0
          84.0       1.2
          98.0       2.2
          99.0       3.0
         112.0       1.5
         126.0       1.0
         128.0       2.8
         140.0       2.9
         142.0      17.2
         143.0       1.8
         212.0       1.3
         224.0       6.4
         225.0       1.1
         226.0     100.0
         227.0      17.0
         228.0       1.3
         252.0       2.8
         310.0       2.0
         311.0       3.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C28 H60 I N 0.036 g : 0.5 ml CDCl3
    tetraheptylammonium iodide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.360 B 1.692 C 1.40 D 1.29 E 0.887

         Hz     ppm     Int.
    

       1351.32   3.382    174
       1345.70   3.368    137
       1343.02   3.361    160
       1339.84   3.353    133
       1334.35   3.339    182
        691.77   1.731     41
        684.45   1.713    104
        683.47   1.711    103
        677.37   1.695    141
        669.80   1.676    118
        661.50   1.656     54
        579.83   1.451     35
        570.92   1.429    102
        565.43   1.415    164
        560.06   1.402    254
        557.13   1.395    255
        556.88   1.394    255
        554.44   1.388    271
        539.92   1.351    109
        532.35   1.333    109
        526.61   1.318    161
        524.54   1.313    173
        520.14   1.302    304
        517.94   1.296    464
        515.14   1.289    405
        511.23   1.280    310
        361.45   0.905    363
        354.61   0.888   1000
        347.66   0.870    393
    

in CDCl3



KBr disc



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