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MS-KW-0166 ethyl 2,5-dichlorobenzoate C9H8Cl2O2 (Mass of molecular ion: 218)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 1.3 27.0 5.7 28.0 3.2 29.0 9.7 36.0 2.1 38.0 1.0 45.0 11.2 50.0 3.4 73.0 2.0 74.0 9.2 75.0 10.2 84.0 2.4 85.0 1.9 99.0 1.0 109.0 13.6 110.0 5.7 111.0 6.3 112.0 2.0 138.0 1.0 139.0 1.5 145.0 22.1 146.0 2.6 147.0 14.3 148.0 1.5 149.0 2.4 173.0 100.0 174.0 11.8 175.0 64.8 176.0 7.7 177.0 10.9 178.0 1.2 183.0 5.7 185.0 1.9 190.0 27.5 191.0 2.4 192.0 17.7 193.0 1.6 194.0 3.0 217.0 1.8 218.0 22.1 219.0 3.4 220.0 14.3 221.0 1.6 222.0 2.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H8 Cl2 O2 0.05 ml : 0.5 ml CDCl3 ethyl 2,5-dichlorobenzoate Assign. Shift(ppm)
A 7.789 B 7.36 C 4.400 D 1.402
Hz ppm Int.
3114.38 7.793 288 3112.92 7.790 391 3111.33 7.786 289 2942.38 7.363 877 2940.92 7.359 668 1769.41 4.428 214 1762.21 4.410 561 1755.13 4.392 576 1747.92 4.374 213 567.50 1.420 595 564.94 1.414 42 564.70 1.413 42 564.33 1.413 43 560.42 1.403 1000 556.15 1.392 35 553.22 1.385 578
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