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(4S,5S)-2,2-dimethyl-4-phenyl-1,3-dioxan-5-amine

产品名称 (4S,5S)-2,2-dimethyl-4-phenyl-1,3-dioxan-5-amine

CAS号35019-66-0

分子式C12H17NO2

分子量207.27


  • Mass

    MS-NW-7612          
    (4S,5S)-(+)-2,2-dimethyl-4-phenyl-1,3-dioxan-5-amine
    C12H17NO2           (Mass of molecular ion:    207)
    

       Source Temperature: 240 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       1.7
          18.0       1.7
          27.0       1.1
          28.0       2.0
          29.0       1.2
          30.0       1.8
          39.0       2.1
          41.0       2.2
          42.0       6.9
          43.0     100.0
          44.0       4.4
          50.0       1.0
          51.0       2.6
          58.0       2.2
          59.0       1.5
          63.0       1.0
          65.0       1.5
          77.0       4.9
          78.0       1.1
          79.0       1.0
          83.0       1.4
          89.0       1.4
          90.0       1.9
          91.0       6.8
          92.0       1.5
         100.0       1.2
         101.0       3.9
         103.0       2.6
         104.0       1.4
         105.0       2.8
         106.0       1.4
         117.0       2.5
         118.0       3.9
         119.0       5.3
         120.0       1.9
         130.0       1.3
         131.0       1.0
         132.0       5.2
         133.0       1.2
         144.0       1.7
         149.0       1.1
         159.0       1.3
         192.0       1.2
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C12 H17 N O2 0.05 ml : 0.5 ml CDCl3
    (4S,5S)-(+)-2,2-dimethyl-4-phenyl-1,3-dioxan-5-amine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.39 to 7.18 B 5.061 C *1 4.238 D *1 3.871 E 2.704 F 1.520 G 1.44 J(B,E)=1.8HZ J(C,D)=-11.7HZ J(C,E)=1.8HZ J(D,E)=2.3HZ

         Hz     ppm     Int.
    

        662.00   7.392     31
        659.38   7.363     71
        657.56   7.343    116
        654.94   7.313    591
        648.13   7.237     35
        646.13   7.215     30
        646.00   7.214     30
        454.25   5.073     94
        452.44   5.052     92
        388.31   4.336     42
        386.00   4.310     44
        376.63   4.206     80
        374.31   4.180     78
        351.81   3.929     87
        350.00   3.908     88
        340.13   3.798     49
        338.31   3.778     49
        245.19   2.738     39
        243.31   2.717     86
        241.13   2.693     82
        239.19   2.671     37
        136.19   1.521   1000
        128.75   1.438    294
    

in CDCl3



liquid film