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网站主页CAS数据库列表 34824-20-9更多图谱1,8-双(羟甲基)蒽(34824-20-9)核磁图(13CNMR)

1,8-双(羟甲基)蒽

产品名称 1,8-双(羟甲基)蒽

CAS号34824-20-9

分子式C16H14O2

分子量238.28

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  • Mass

    MS-KW-0566          
    1,8-anthracenedimethanol
    C16H14O2            (Mass of molecular ion:    238)
    

       Source Temperature: 170 °C
       Sample Temperature: 160 °C
       Direct, 75 eV
    

          17.0       1.3
          18.0       6.9
          28.0       1.2
          39.0       1.2
          51.0       1.4
          63.0       2.4
          74.0       1.3
          75.0       2.6
          76.0       4.4
          77.0       1.1
          81.0       1.0
          81.5       2.1
          82.0       2.5
          82.5       4.5
          83.0       1.6
          87.0       1.7
          88.0       4.5
          88.5       1.2
          89.0       4.4
          93.5       1.8
          94.0       2.5
          94.5       6.8
          95.0       5.9
          95.5       4.2
          96.0       4.9
          97.0       1.7
         100.0       1.0
         101.0       1.7
         102.5       1.6
         103.0       1.5
         104.0       1.9
         104.5       1.1
         109.0       5.5
         109.5       2.6
         110.0       7.7
         110.5       1.5
         115.0       1.4
         118.0       1.0
         126.0       1.1
         139.0       1.7
         150.0       2.8
         151.0       4.3
         152.0       5.1
         153.0       1.1
         163.0       3.1
         164.0       1.7
         165.0       8.6
         166.0       2.0
         174.0       1.3
         175.0       1.7
         176.0       8.9
         177.0       6.7
         178.0      29.8
         179.0      25.2
         180.0       4.0
         187.0       3.1
         188.0       2.9
         189.0      24.6
         190.0      16.2
         191.0      68.5
         192.0      32.8
         193.0       6.4
         194.0       1.5
         201.0       1.4
         202.0       3.4
         203.0       2.7
         204.0       1.7
         205.0       4.9
         206.0       5.7
         207.0       4.6
         208.0       1.6
         209.0       1.8
         218.0       1.1
         219.0      23.0
         220.0      31.8
         221.0      14.8
         222.0       6.9
         223.0       1.3
         236.0       4.3
         237.0       1.7
         238.0     100.0
         239.0      17.5
         240.0       1.8
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C16H14O2 0.030 g : 0.5 ml DMSO-d6
    1,8-anthracenedimethanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.776 B 8.580 C 7.979 D 7.591 E 7.483 F 5.44 G 5.155

         Hz     ppm     Int.
    

       3508.31   8.776    124
       3429.94   8.580    156
       3194.10   7.990    121
       3185.55   7.969    131
       3038.82   7.602     99
       3037.85   7.599    105
       3032.11   7.585    139
       3031.13   7.582    139
       3002.57   7.511    147
       2995.85   7.494    114
       2994.15   7.490    143
       2987.43   7.473     99
       2180.91   5.456    123
       2175.30   5.442    306
       2169.80   5.428    146
       2063.36   5.162    283
       2057.87   5.148    254
       1368.54   3.424   1000
    

in DMSO-d6



KBr disk



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