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网站主页CAS数据库列表 348-52-7更多图谱2-氟碘苯(348-52-7)核磁图(1HNMR)

2-氟碘苯

产品名称 2-氟碘苯

CAS号348-52-7

分子式C6H4FI

分子量222

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  • Mass

    MS-NW-9350          
    o-fluoroiodobenzene
    C6H4FI              (Mass of molecular ion:    222)
    

       Source Temperature: 280 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          31.0       1.2
          37.0       1.1
          38.0       1.2
          39.0       1.2
          50.0       7.2
          51.0       3.3
          62.0       1.0
          63.0       1.0
          68.0       4.8
          69.0       5.2
          74.0       4.0
          75.0      24.8
          76.0       2.2
          93.0       1.3
          94.0       5.4
          95.0      65.9
          96.0       4.5
         111.0       4.5
         127.0       2.0
         222.0     100.0
         223.0       6.6
    

400 MHz in CDCl3

parameter in CCl4


  • 1H NMR 399.65 MHz
    C6 H4 F I 0.05 ml : 0.5 ml CDCl3
    o-fluoroiodobenzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.713 B 7.275 C 7.029 D 6.865

         Hz     ppm     Int.
    

       3090.70   7.734    481
       3089.11   7.730    497
       3084.35   7.718    507
       3082.76   7.714    934
       3081.18   7.710    587
       3076.42   7.698    530
       3074.83   7.694    553
       2919.31   7.305    242
       2917.72   7.301    253
       2914.18   7.292    260
       2912.48   7.288    346
       2911.99   7.287    357
       2911.13   7.285    373
       2910.28   7.283    353
       2909.42   7.280    339
       2906.86   7.274    321
       2906.01   7.272    364
       2905.15   7.270    369
       2904.30   7.268    434
       2903.69   7.266    408
       2902.10   7.262    343
       2898.56   7.253    346
       2896.97   7.249    324
       2817.87   7.051    521
       2816.41   7.048    575
       2813.72   7.041     36
       2809.57   7.031    903
       2808.23   7.027   1000
       2805.54   7.020     54
       2804.08   7.017     36
       2801.39   7.010    469
       2800.05   7.007    489
       2752.08   6.887    559
       2750.61   6.883    553
       2744.51   6.868    762
       2743.04   6.864    794
       2736.82   6.849    523
       2735.35   6.845    520
    


  • 1H NMR 300 MHz
    C6 H4 F I 10 vol% in CCl4
    o-fluoroiodobenzene
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 7.70 D(B) 6.84 D(C) 7.25 D(D) 7.00 D(X) 20.95 J(A,B) 7.83 J(A,C) 1.64 J(A,D) 0.26 J(A,X) 6.30 J(B,C) 7.39 J(B,D) 1.43 J(B,X) -0.24 J(C,D) 8.22 J(C,X) 5.03 J(D,X) 7.94 ROARK,J.L. & SMITH,W.B. J.PHYS.CHEM. 73, 1046 (1969) F-19 REFERENCE : 1,1,2,2-TETRACHLORO-3,3,4,4-TETRAFLUOROCYCLOBUTANE

         Hz     ppm     Int.
    

       2317.93   7.726    479
       2316.31   7.721    492
       2311.56   7.705    543
       2310.05   7.700   1000
       2308.51   7.695    560
       2303.76   7.679    507
       2302.15   7.674    533
       2186.46   7.288    239
       2184.83   7.283    238
       2181.32   7.271    269
       2179.61   7.265    361
       2179.13   7.264    395
       2178.24   7.261    401
       2177.48   7.258    368
       2176.62   7.255    350
       2173.89   7.246    336
       2173.24   7.244    391
       2172.27   7.241    384
       2171.65   7.239    426
       2170.92   7.236    417
       2169.24   7.231    343
       2165.79   7.219    340
       2164.21   7.214    328
       2108.59   7.029    541
       2107.15   7.024    580
       2100.51   7.002    934
       2099.02   6.997    990
       2092.57   6.975    458
       2090.96   6.970    476
       2060.11   6.867    470
       2058.75   6.862    519
       2052.62   6.842    825
       2051.16   6.837    862
       2045.06   6.817    438
       2043.52   6.812    462
    

in CDCl3



liquid film