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网站主页CAS数据库列表 3446-90-0更多图谱对甲硫基苯甲醇(3446-90-0)核磁图(1HNMR)

对甲硫基苯甲醇

产品名称 对甲硫基苯甲醇

CAS号3446-90-0

分子式C8H10OS

分子量154.23

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  • Mass

    MS-IW-0096          
    p-(methylthio)benzyl alcohol
    C8H10OS             (Mass of molecular ion:    154)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       1.1
          27.0       1.4
          29.0       1.3
          31.0       1.3
          38.0       1.0
          39.0       4.6
          41.0       1.0
          45.0      10.9
          47.0       1.6
          50.0       4.0
          51.0       7.7
          52.0       1.7
          53.0       1.6
          58.0       1.4
          62.0       1.7
          63.0       4.2
          65.0       4.6
          66.0       3.1
          67.0       1.9
          69.0       4.9
          71.0       1.4
          74.0       1.7
          75.0       2.9
          76.0       2.0
          77.0      24.5
          78.0      10.2
          79.0      34.5
          80.0       2.4
          82.0       1.9
          84.0       1.0
          89.0       2.5
          91.0       5.1
          95.0       1.1
         105.0       3.8
         106.0       1.0
         107.0      35.0
         108.0       5.6
         109.0      24.3
         110.0      10.9
         111.0       4.7
         121.0       5.3
         122.0      10.1
         123.0       5.6
         124.0       2.1
         125.0      20.1
         126.0       2.1
         127.0       1.0
         135.0       2.0
         136.0       1.0
         137.0      29.4
         138.0       4.6
         139.0       5.7
         151.0       9.3
         152.0       7.6
         153.0      20.5
         154.0     100.0
         155.0      10.6
         156.0       5.3
         168.0       1.3
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H10 O S 0.033 g : 0.5 ml CDCl3
    p-(methylthio)benzyl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 7.245 B *1 7.229 C 4.591 D 2.464 E 2.20

         Hz     ppm     Int.
    

       2902.71   7.264     49
       2900.51   7.258     54
       2896.73   7.249     47
       2894.17   7.242    332
       2891.11   7.235    397
       2888.43   7.228     65
       2885.01   7.219     33
       2883.30   7.215     44
       2882.45   7.213     60
       1835.08   4.592    249
        984.86   2.465   1000
        878.66   2.199     39
    

in CDCl3



KBr disc



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