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MS-IW-6467 N-acetonylphthalimide C11H9NO3 (Mass of molecular ion: 203)
Source Temperature: 140 °C Sample Temperature: 110 °C Direct, 75 eV
43.0 6.6 50.0 3.8 51.0 2.4 66.0 1.0 74.0 1.6 75.0 2.4 76.0 8.8 77.0 10.2 78.0 1.1 104.0 9.2 105.0 5.1 117.0 2.4 130.0 1.6 132.0 3.6 133.0 10.5 160.0 100.0 161.0 78.0 162.0 8.1 203.0 21.4 204.0 3.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H9 N O3 0.040 g : 0.5 ml CDCl3 N-acetonylphthalimide Assign. Shift(ppm)
A 7.868 B 7.742 C 4.510 D 2.272
Hz ppm Int.
3152.83 7.889 22 3149.05 7.880 208 3146.00 7.872 206 3143.80 7.867 159 3143.43 7.866 165 3140.63 7.859 273 3136.60 7.849 31 3135.50 7.846 26 3103.52 7.766 28 3102.29 7.763 36 3098.39 7.753 268 3095.46 7.746 163 3092.90 7.740 199 3089.84 7.732 214 1802.37 4.510 641 908.20 2.273 1000 905.03 2.265 28
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