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网站主页CAS数据库列表 34071-95-9更多图谱羟苯基丙酸N-羟基琥珀酰亚胺酯(34071-95-9)质谱(MS)

羟苯基丙酸N-羟基琥珀酰亚胺酯

产品名称 羟苯基丙酸N-羟基琥珀酰亚胺酯

CAS号34071-95-9

分子式C13H13NO5

分子量263.25

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  • Mass

    MS-NW-5474          
    N-(3-(p-hydroxyphenyl)propionyloxy)succinimide
    C13H13NO5           (Mass of molecular ion:    263)
    

       Source Temperature: 180 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          14.0       1.5
          15.0       1.7
          26.0       6.1
          27.0      15.8
          28.0      23.6
          29.0       6.1
          30.0       1.9
          31.0       3.3
          38.0       1.5
          39.0       7.5
          40.0       1.3
          41.0       1.9
          42.0       7.7
          43.0       6.4
          44.0       1.8
          45.0       6.4
          50.0       1.7
          51.0       4.3
          52.0       1.9
          53.0       2.7
          54.0       1.0
          55.0      28.4
          56.0       5.8
          57.0       2.2
          59.0       4.7
          62.0       1.2
          63.0       2.9
          65.0       5.2
          66.0       1.1
          70.0       2.6
          73.0       3.0
          74.0       5.3
          77.0      12.3
          78.0       2.8
          79.0       1.7
          87.0      12.0
          91.0       5.7
          94.0       2.1
         100.0       1.9
         101.0       1.1
         103.0       1.5
         107.0     100.0
         108.0       7.4
         115.0      16.1
         119.0       2.4
         120.0       7.5
         121.0       2.0
         123.0       1.2
         166.0      26.4
         167.0       2.6
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C13 H13 N O5 0.015 g : 0.5 ml CDCl3
    N-(3-(p-hydroxyphenyl)propionyloxy)succinimide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.06 B 6.77 C 5. D 3.00 to 2.86 E 2.828

         Hz     ppm     Int.
    

        638.25   7.127    116
        636.88   7.112     61
        636.25   7.105     59
        631.88   7.056     62
        629.56   7.030    213
        609.81   6.809    254
        607.94   6.789     97
        607.63   6.785     98
        603.31   6.737     62
        601.13   6.713    141
        265.88   2.969    103
        265.56   2.966    103
        261.81   2.924    234
        260.19   2.906    256
        257.63   2.877    120
        256.50   2.865    184
        253.38   2.830   1000
        250.44   2.797    105
        249.75   2.789     99
        249.19   2.783    102
    


  • 1H NMR 399.65 MHz
    C13 H13 N O5 saturated in CDCl3
    N-(3-(p-hydroxyphenyl)propionyloxy)succinimide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.078 B 6.771 C 5.4 D 2.97 E 2.86 F 2.84

         Hz     ppm     Int.
    

       2843.75   7.116     31
       2843.14   7.115     33
       2841.43   7.110     40
       2840.45   7.108     44
       2839.60   7.106     46
       2838.75   7.104     53
       2832.89   7.089    630
       2824.46   7.068    714
       2817.63   7.051     35
       2817.38   7.050     35
       2816.28   7.047     32
       2719.60   6.805     30
       2717.90   6.801     41
       2716.80   6.798     48
       2716.31   6.797     51
       2715.94   6.796     53
       2713.01   6.789    158
       2710.21   6.782    841
       2708.13   6.777    342
       2705.69   6.771    120
       2703.61   6.765    307
       2701.66   6.761    752
       2698.85   6.754    131
       2695.56   6.745     40
       1211.43   3.032     30
       1210.57   3.030     32
       1210.21   3.029     33
       1209.84   3.028     33
       1209.23   3.026     34
       1208.62   3.025     35
       1207.52   3.022     35
       1206.79   3.020     36
       1206.42   3.019     39
       1206.05   3.018     38
       1205.32   3.016     41
       1204.71   3.015     40
       1204.10   3.013     41
       1203.49   3.012     47
       1203.25   3.011     47
       1201.90   3.008     55
       1201.54   3.007     56
       1200.93   3.005     62
       1195.80   2.993    235
       1188.84   2.975    491
       1180.79   2.955    463
       1177.00   2.946     70
       1175.90   2.943     59
       1175.29   2.941     55
       1174.93   2.940     54
       1174.32   2.939     55
       1173.46   2.937     63
       1173.10   2.936     64
       1171.88   2.933     58
       1171.39   2.932     60
       1171.14   2.931     60
       1170.78   2.930     61
       1170.17   2.928     63
       1169.68   2.927     60
       1169.31   2.926     58
       1168.58   2.925     56
       1167.85   2.923     56
       1167.48   2.922     55
       1166.99   2.921     56
       1166.50   2.919     58
       1164.67   2.915     65
       1163.94   2.913     72
       1163.45   2.912     77
       1162.96   2.910     81
       1160.40   2.904    112
       1159.55   2.902    107
       1158.69   2.900    109
       1158.08   2.898    108
       1157.71   2.897    108
       1150.88   2.880    590
       1150.51   2.879    590
       1146.48   2.869    306
       1146.12   2.868    306
       1144.29   2.864    537
       1142.94   2.860    753
       1134.52   2.839   1000
       1123.05   2.811    163
       1122.19   2.808    156
       1121.83   2.808    153
       1121.22   2.806    154
       1116.82   2.795     60
       1115.97   2.793     54
       1114.75   2.790     48
       1114.14   2.788     42
       1113.77   2.787     42
       1113.28   2.786     41
       1112.43   2.784     37
       1111.82   2.782     35
       1111.45   2.782     35
       1110.96   2.780     33
       1110.60   2.779     30
       1110.11   2.778     33
    

in CDCl3



KBr disc