图谱信息 供应商 相关产品
网站主页CAS数据库列表 3404-77-1更多图谱3,3-二甲基-1-己烯(3404-77-1)核磁图(1HNMR)

3,3-二甲基-1-己烯

产品名称 3,3-二甲基-1-己烯

CAS号3404-77-1

分子式C8H16

分子量112.21

展开


  • Mass

    MS-IW-6600          
    3,3-dimethyl-1-hexene
    C8H16               (Mass of molecular ion:    112)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       7.9
          28.0       1.5
          29.0       5.6
          39.0       9.1
          40.0       1.7
          41.0      55.8
          42.0       5.8
          43.0      10.9
          51.0       1.3
          53.0       5.0
          54.0       1.0
          55.0      56.1
          56.0      23.2
          57.0       9.4
          67.0       5.3
          68.0       6.4
          69.0     100.0
          70.0      37.2
          71.0       2.2
          83.0      13.0
          84.0       7.8
          85.0       2.1
          97.0       8.6
         112.0       7.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H16 0.05 ml : 0.5 ml CDCl3
    3,3-dimethyl-1-hexene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.760 B 4.884 C 4.882 D 1.24 E 0.968 F 0.87

         Hz     ppm     Int.
    

       2316.77   5.797    118
       2306.40   5.772    103
       2302.49   5.762     32
       2298.95   5.753    114
       2288.57   5.727    140
       1960.82   4.907     67
       1959.23   4.903    176
       1957.40   4.898    211
       1955.81   4.894     92
       1947.02   4.872     98
       1945.43   4.868    171
       1942.87   4.862    143
       1941.41   4.858     95
        498.41   1.248    113
        494.75   1.238    418
        492.68   1.233    151
        491.94   1.231    168
        490.48   1.228    169
        489.99   1.227    169
        487.06   1.219     56
        485.60   1.216     50
        483.76   1.211     41
        482.18   1.207     34
        386.96   0.969   1000
        354.49   0.888    110
        353.39   0.885     84
        351.93   0.881     96
        349.85   0.876     79
        349.12   0.874     87
        347.53   0.870    276
        345.95   0.866    123
        345.09   0.864    158
        342.90   0.859     79
        341.80   0.856     80
        340.45   0.852    106
    

in CDCl3



liquid film