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MassMS-IW-0059 m-diphenoxybenzene C18H14O2 (Mass of molecular ion: 262)
Source Temperature: 260 °C Sample Temperature: 160 °C Reservoir, 75 eV
39.0 2.2 50.0 1.9 51.0 8.4 63.0 3.4 64.0 4.2 65.0 2.2 75.0 1.1 76.0 1.7 77.0 15.0 78.0 1.4 89.0 1.0 91.0 2.1 92.0 1.8 95.0 1.5 115.0 18.9 116.0 2.2 121.0 5.3 127.0 1.8 128.0 4.7 129.0 2.0 131.0 1.5 139.0 5.4 140.0 4.1 141.0 59.4 142.0 7.6 157.0 2.3 168.0 14.1 169.0 11.2 170.0 1.4 191.0 1.2 193.0 1.0 205.0 1.1 215.0 1.6 219.0 1.3 233.0 3.0 234.0 3.5 261.0 4.3 262.0 100.0 263.0 19.6 264.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C18 H14 O2 0.036 g : 0.5 ml CDCl3 m-diphenoxybenzene 
Assign. Shift(ppm)
A 7.323 B 7.237 C 7.098 D 7.025 E 6.71 F 6.69
Hz ppm Int.2937.50 7.351 91 2935.18 7.345 549 2933.11 7.340 235 2930.18 7.332 127 2928.71 7.329 316 2927.86 7.327 833 2926.64 7.324 787 2924.32 7.318 150 2921.14 7.310 296 2919.19 7.305 777 2916.87 7.299 122 2901.37 7.260 183 2900.76 7.259 186 2892.82 7.239 418 2885.13 7.220 226 2884.64 7.218 235 2844.97 7.119 196 2843.87 7.116 378 2842.65 7.113 238 2837.77 7.101 222 2836.43 7.098 603 2835.69 7.096 315 2834.96 7.094 232 2830.08 7.082 159 2828.98 7.079 296 2827.88 7.076 172 2813.96 7.042 147 2813.35 7.040 163 2812.01 7.037 853 2810.79 7.034 1000 2810.06 7.032 568 2808.72 7.028 281 2805.30 7.020 272 2804.32 7.017 464 2803.22 7.015 855 2802.25 7.012 756 2799.68 7.006 112 2688.23 6.727 567 2685.91 6.721 623 2680.42 6.707 220 2679.69 6.706 272 2677.86 6.701 814 2674.44 6.692 364 2672.61 6.688 397 2670.29 6.682 165
in CDCl3
KBr disc
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