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MS-NW-5588 4-phenyl-1-butanol C10H14O (Mass of molecular ion: 150)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
27.0 3.1 28.0 1.2 29.0 1.2 31.0 6.5 39.0 6.5 41.0 4.9 50.0 1.7 51.0 5.1 52.0 1.4 53.0 1.0 63.0 2.9 65.0 12.1 77.0 6.0 78.0 6.6 79.0 4.3 89.0 2.2 90.0 1.2 91.0 81.2 92.0 11.0 93.0 1.1 103.0 3.6 104.0 100.0 105.0 12.1 106.0 1.5 115.0 3.6 116.0 1.4 117.0 24.5 118.0 2.5 131.0 4.1 132.0 12.4 133.0 1.4 150.0 19.2 151.0 2.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H14 O 0.04 ml : 0.5 ml CDCl3 4-phenyl-1-butanol Assign. Shift(ppm)
A 7.27 to 7.14 B 3.619 C 2.62 D 1.68 to 1.56
Hz ppm Int.
658.44 7.352 93 655.75 7.322 47 655.25 7.317 48 653.13 7.293 72 650.63 7.265 178 648.00 7.236 208 645.94 7.213 1000 644.38 7.195 977 641.00 7.158 158 640.50 7.152 139 639.19 7.138 90 638.44 7.129 113 637.75 7.121 71 636.88 7.112 103 631.88 7.056 47 330.44 3.690 200 328.69 3.671 75 326.94 3.651 55 326.44 3.645 68 324.13 3.620 627 322.13 3.597 144 320.38 3.578 83 317.94 3.551 205 242.88 2.712 83 240.94 2.691 53 240.38 2.685 50 240.19 2.682 50 238.06 2.659 110 235.75 2.633 251 233.38 2.606 88 232.19 2.593 65 231.31 2.583 67 228.63 2.553 161 160.31 1.790 86 155.94 1.742 97 153.56 1.715 136 151.94 1.697 124 149.06 1.665 433 146.19 1.633 929 143.75 1.606 189 142.31 1.589 490 139.63 1.560 157 137.31 1.534 75 134.94 1.507 69 132.00 1.474 54 127.75 1.427 46
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