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MS-IW-3475 1,3-dichloro-2-(methoxymethyl)benzene C8H8Cl2O (Mass of molecular ion: 190)
Source Temperature: 210 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 1.2 29.0 4.7 37.0 1.0 38.0 1.2 39.0 3.0 43.0 1.1 44.0 1.9 45.0 8.3 50.0 3.5 51.0 3.3 61.0 2.1 62.0 4.9 63.0 8.9 73.0 5.4 74.0 4.0 75.0 10.2 76.0 1.2 77.0 2.5 84.0 1.3 85.0 1.9 86.0 1.8 87.0 2.3 88.0 1.0 89.0 15.8 90.0 2.0 91.0 11.1 92.0 1.3 97.0 2.0 99.0 3.4 105.0 1.3 109.0 2.4 110.0 1.2 111.0 10.2 112.0 1.8 113.0 3.2 123.0 9.3 124.0 4.4 125.0 10.0 126.0 2.3 127.0 2.5 133.0 2.1 135.0 1.3 139.0 4.1 141.0 1.4 145.0 1.5 147.0 2.0 155.0 100.0 156.0 9.0 157.0 33.0 158.0 3.0 159.0 78.7 160.0 6.4 161.0 50.8 162.0 4.1 163.0 8.4 173.0 2.8 175.0 2.4 189.0 6.0 190.0 21.0 191.0 5.7 192.0 13.6 193.0 1.8 194.0 2.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H8 Cl2 O 0.05 ml : 0.5 ml CDCl3 1,3-dichloro-2-(methoxymethyl)benzene Assign. Shift(ppm)
A 7.286 B 7.145 C 4.704 D 3.421
Hz ppm Int.
2916.14 7.297 307 2910.89 7.284 31 2907.96 7.277 440 2862.55 7.163 200 2855.10 7.145 173 2854.00 7.142 163 2846.44 7.123 122 1880.25 4.705 675 1367.43 3.422 1000
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