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3,5-二溴-4-羟基苯甲酸

产品名称 3,5-二溴-4-羟基苯甲酸

CAS号3337-62-0

分子式C7H4Br2O3

分子量295.91

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  • Mass

    MS-IW-0060          
    3,5-dibromo-4-hydroxybenzoic acid
    C7H4Br2O3           (Mass of molecular ion:    294)
    

       Source Temperature: 210 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       1.0
          37.0       1.4
          45.0       1.3
          51.0       2.6
          53.0       3.4
          61.0       4.3
          62.0       8.3
          63.0       6.3
          79.0       1.9
          80.0       1.0
          85.0       1.3
          86.0       1.1
          90.0       4.1
          91.0       3.0
         119.0       1.0
         133.0       2.3
         134.0       3.2
         135.0       1.7
         139.5       1.0
         141.0       1.8
         142.0       1.1
         143.0       2.2
         169.0       2.0
         170.0       4.4
         171.0       2.4
         172.0       4.3
         197.0       1.7
         199.0       1.8
         221.0       1.1
         223.0       2.1
         225.0       1.0
         249.0       3.4
         250.0       1.2
         251.0       6.7
         252.0       1.3
         253.0       3.3
         277.0      31.7
         278.0       2.8
         279.0      61.9
         280.0       5.0
         281.0      30.6
         282.0       2.3
         294.0      50.9
         295.0       4.5
         296.0     100.0
         297.0       8.1
         298.0      49.3
         299.0       3.9
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C7 H4 Br2 O3 0.031 g : 0.5 ml DMSO-d6
    3,5-dibromo-4-hydroxybenzoic acid
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 13. B *1 11. C 8.029

         Hz     ppm     Int.
    

       3212.95   8.040     20
       3209.11   8.030   1000
       3205.26   8.021     22
    

in DMSO-d6



KBr disc



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