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网站主页CAS数据库列表 33183-07-2更多图谱环己烯基二茂铁(33183-07-2)质谱(MS)

环己烯基二茂铁

产品名称 环己烯基二茂铁

CAS号33183-07-2

分子式C16H9Fe

分子量257.09

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  • Mass

    MS-IW-4169          
    (1-cyclohexenyl)ferrocene
    C16H18Fe            (Mass of molecular ion:    266)
    

       Source Temperature: 130 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          56.0       6.8
         115.0       2.7
         116.0       1.3
         121.0       7.7
         122.0       1.2
         125.5       2.3
         128.0       1.4
         133.0       1.1
         134.0       1.7
         141.0       2.7
         142.0       2.2
         171.0       1.1
         172.0       4.0
         186.0       1.9
         196.0       2.8
         197.0       2.5
         198.0       6.4
         199.0       2.6
         200.0       1.1
         212.0       1.4
         223.0       1.0
         236.0       1.8
         237.0       1.1
         238.0      13.0
         239.0       2.3
         262.0       4.2
         263.0       2.0
         264.0       8.4
         265.0       3.8
         266.0     100.0
         267.0      19.9
         268.0       2.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C16 H18 Fe 0.034 g : 0.5 ml CDCl3
    (1-cyclohexenyl)ferrocene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.886 B 4.312 C 4.147 D 4.077 E 2.318 F 2.039 G 1.736 J 1.633

         Hz     ppm     Int.
    

       2356.45   5.897     33
       2354.25   5.891     44
       2352.54   5.887     62
       2350.83   5.883     45
       2348.63   5.877     34
       1725.34   4.318    134
       1723.51   4.313    208
       1721.68   4.308    153
       1659.42   4.153    151
       1657.47   4.148    211
       1655.64   4.143    144
       1629.64   4.078   1000
        934.33   2.338     36
        932.25   2.333     44
        930.30   2.328     50
        928.22   2.323     74
        926.39   2.319     76
        924.32   2.313     56
        922.12   2.308     49
        920.29   2.303     44
        820.43   2.053     56
        817.99   2.047     70
        816.41   2.043     59
        814.21   2.038     74
        811.89   2.032     58
        808.11   2.023     36
        700.68   1.754     50
        697.39   1.746     48
        695.07   1.740     73
        691.41   1.731     51
        689.21   1.725     72
        683.11   1.710     31
        663.70   1.661     32
        657.84   1.647     74
        655.64   1.641     53
        651.98   1.632     73
        649.66   1.626     49
        646.48   1.618     48
    

in CDCl3



KBr disc



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