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网站主页CAS数据库列表 3294-03-9更多图谱2,2'-硫代双(4-特辛基苯酚)(3294-03-9)质谱(MS)

2,2'-硫代双(4-特辛基苯酚)

产品名称 2,2'-硫代双(4-特辛基苯酚)

CAS号3294-03-9

分子式C28H42O2S

分子量442.7

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  • Mass

    MS-IW-9464          
    2,2'-thiobis(4-(1,1,3,3-tetramethylbutyl)phenol)
    C28H42O2S           (Mass of molecular ion:    442)
    

       Source Temperature: 170 °C
       Sample Temperature: 160 °C
       Direct, 75 eV
    

          18.0       3.2
          27.0       1.8
          28.0       1.2
          29.0       9.9
          39.0       2.2
          41.0      16.7
          43.0      12.9
          45.0       1.7
          53.0       1.4
          55.0       5.6
          56.0       1.4
          57.0      64.7
          58.0       2.8
          59.0       1.9
          65.0       1.4
          69.0       1.5
          71.0       3.1
          77.0       3.0
          78.0       1.0
          79.0       2.7
          91.0       4.4
          93.0       2.2
          94.0       1.5
          95.0       2.2
          97.0       2.7
         103.0       2.3
         104.0       1.4
         105.0       4.5
         106.0       1.0
         107.0       7.2
         113.0       1.3
         115.0       1.2
         117.0       1.0
         119.0       4.0
         120.0       1.0
         121.0       2.5
         122.0       6.3
         123.0       1.4
         125.0       3.1
         128.0       1.2
         131.0       1.2
         132.0       1.3
         133.0       8.3
         134.0      13.2
         135.0      24.7
         136.0       9.4
         136.5       1.2
         137.0       6.4
         138.0       3.3
         139.0       2.4
         146.0       1.0
         147.0       2.9
         148.0       3.0
         149.0       2.9
         149.5       3.5
         150.0      29.9
         150.5       5.0
         151.0       5.3
         152.0       1.0
         165.0      14.5
         166.0      18.8
         167.0      12.0
         168.0       2.2
         179.0       2.9
         180.0       2.1
         181.0       3.6
         231.0       1.3
         237.0       1.1
         259.0      53.6
         260.0       9.2
         261.0       3.4
         273.0       1.2
         299.0       4.9
         300.0       1.2
         313.0       1.0
         371.0     100.0
         372.0      26.4
         373.0       8.1
         374.0       1.5
         442.0       7.8
         443.0       2.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C28 H42 O2 S 0.039 g : 0.5 ml CDCl3
    2,2'-thiobis(4-(1,1,3,3-tetramethylbutyl)phenol)
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.309 B 7.208 C 6.860 D 6.20 E 1.622 F 1.260 G 0.656

         Hz     ppm     Int.
    

       2922.24   7.312     84
       2919.92   7.307     93
       2886.60   7.223     46
       2884.16   7.217     40
       2878.05   7.202     51
       2875.61   7.196     46
       2745.48   6.870     98
       2736.94   6.849     88
       2478.39   6.202    153
        648.19   1.622    240
        503.78   1.261    604
        262.21   0.657   1000
    

in CDCl3



KBr disc



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