图谱信息 供应商 相关产品
网站主页CAS数据库列表 328-70-1更多图谱3,5-双三氟甲基溴苯(328-70-1)质谱(MS)

3,5-双三氟甲基溴苯

产品名称 3,5-双三氟甲基溴苯

CAS号328-70-1

分子式C8H3BrF6

分子量293

展开


  • Mass

    MS-IW-8120          
    1-bromo-3,5-bis(trifluoromethyl)benzene
    C8H3BrF6            (Mass of molecular ion:    292)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          31.0       1.2
          50.0       2.9
          57.0       1.0
          62.0       1.1
          69.0       6.3
          73.0       1.3
          74.0       6.7
          75.0      10.7
          87.0       1.1
          93.0       2.3
          94.0       2.9
          99.0       3.5
         113.0       1.7
         123.0       2.3
         124.0       1.0
         125.0       6.3
         143.0      12.7
         144.0      16.6
         145.0       1.7
         162.0       4.2
         163.0      22.9
         164.0       1.9
         193.0       5.7
         194.0       9.6
         195.0       1.4
         212.0       2.2
         213.0      78.4
         214.0       7.6
         223.0       5.9
         225.0       5.9
         242.0       5.3
         244.0       5.1
         273.0      22.6
         274.0       2.3
         275.0      22.2
         276.0       2.0
         291.0       1.2
         292.0     100.0
         293.0       9.9
         294.0      97.2
         295.0       8.6
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H3 Br F6 0.05 ml : 0.5 ml CDCl3
    1-bromo-3,5-bis(trifluoromethyl)benzene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.962 B 7.827

         Hz     ppm     Int.
    

       3182.13   7.963   1000
       3181.64   7.962    999
       3128.78   7.829    415
       3128.05   7.827    462
       3127.44   7.826    432
    

in CDCl3



liquid film