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MassMS-NW-6651 (diacetoxyiodo)benzene C10H11IO4 (Mass of molecular ion: 322)
Source Temperature: 160 °C Sample Temperature: 100 °C Direct, 75 eV
15.0 3.9 27.0 1.2 28.0 1.0 38.0 1.0 39.0 1.5 42.0 1.4 43.0 11.3 44.0 4.7 45.0 4.4 50.0 10.4 51.0 22.7 52.0 1.1 60.0 3.8 63.0 1.3 65.0 2.2 74.0 3.7 75.0 2.3 76.0 4.1 77.0 73.5 78.0 5.1 94.0 3.6 102.0 1.9 107.0 3.4 109.0 1.4 122.0 2.5 124.0 1.1 127.0 2.3 166.0 2.7 168.0 1.3 204.0 100.0 205.0 6.8 263.0 41.1 264.0 3.8
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H11 I O4 0.040 g : 0.5 ml DMSO-d6 (diacetoxyiodo)benzene 
Assign. Shift(ppm)
A 8.238 B 7.675 C 7.575 D 1.916
Hz ppm Int.3297.12 8.251 79 3296.02 8.248 86 3290.65 8.234 25 3288.82 8.230 100 3287.60 8.227 79 3076.17 7.698 20 3068.73 7.679 54 3062.50 7.663 24 3061.40 7.661 40 3060.30 7.658 22 3034.18 7.593 75 3032.71 7.589 34 3026.37 7.573 111 3018.92 7.554 51 765.87 1.917 1000
in DMSO-d6
KBr disc
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