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MassMS-IW-6461 2,2'-methylenebis(p-cresol) C15H16O2 (Mass of molecular ion: 228)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 1.7 39.0 1.5 51.0 1.7 53.0 1.3 55.0 1.0 63.0 1.0 65.0 2.3 76.0 1.3 77.0 5.8 78.0 1.4 79.0 1.9 89.0 1.7 90.0 1.7 91.0 7.3 92.0 2.8 93.0 1.6 97.0 2.0 99.0 1.2 104.0 3.3 105.0 2.1 106.0 1.2 107.0 12.2 108.0 71.5 109.0 5.5 113.0 3.4 114.0 5.0 115.0 2.0 119.0 2.1 120.0 4.0 121.0 100.0 122.0 9.9 128.0 1.3 141.0 1.2 145.0 1.0 152.0 1.9 153.0 1.2 165.0 5.2 166.0 3.5 167.0 1.4 181.0 1.7 195.0 6.8 196.0 1.4 197.0 1.3 208.0 1.0 209.0 4.7 210.0 1.7 211.0 2.3 212.0 1.2 213.0 2.1 227.0 4.8 228.0 95.2 229.0 15.7 230.0 1.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C15 H16 O2 0.038 g : 0.5 ml CDCl3 2,2'-methylenebis(p-cresol) 
Assign. Shift(ppm)
A 7.67 B 7.070 C 6.836 D 6.685 E 3.837 F 2.237
Hz ppm Int.3065.31 7.670 484 2826.66 7.073 195 2824.58 7.068 196 2737.67 6.851 97 2737.18 6.849 96 2735.47 6.845 95 2729.49 6.830 119 2729.00 6.829 119 2727.42 6.825 115 2675.17 6.694 281 2666.99 6.674 219 1533.57 3.838 321 894.04 2.238 1000
in CDCl3
KBr disc
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