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网站主页CAS数据库列表 321-60-8更多图谱2-氟联苯(321-60-8)核磁图(13CNMR)

2-氟联苯

产品名称 2-氟联苯

CAS号321-60-8

分子式C12H9F

分子量172.2

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  • Mass

    MS-NW-6602          
    2-fluorobiphenyl
    C12H9F              (Mass of molecular ion:    172)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          39.0       1.6
          50.0       2.4
          51.0       3.0
          57.0       1.0
          62.0       1.2
          63.0       2.8
          73.0       3.2
          74.0       2.4
          75.0       3.3
          76.0       3.1
          85.0       6.2
          85.5       1.1
          86.0       4.0
          94.0       1.4
          99.0       1.3
         107.0       1.0
         120.0       2.9
         125.0       1.7
         126.0       1.1
         133.0       4.1
         144.0       1.8
         145.0       1.2
         146.0       4.9
         150.0       1.8
         151.0       3.8
         152.0       4.8
         153.0       1.6
         157.0       1.5
         168.0       1.0
         169.0       3.4
         170.0      18.4
         171.0      27.7
         172.0     100.0
         173.0      12.8
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H9 F 0.051 g : 0.5 ml CDCl3
    2-fluorobiphenyl
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.543 B 7.45 to 7.40 C 7.355 D 7.286 E 7.186 G 7.135

         Hz     ppm     Int.
    

       3026.49   7.573     30
       3024.41   7.568     34
       3020.87   7.559    297
       3019.29   7.555    584
       3017.70   7.551    449
       3015.63   7.546    150
       3014.16   7.543    186
       3013.55   7.541    221
       3012.45   7.538    528
       3011.84   7.537    446
       3010.99   7.535    588
       3009.40   7.531    383
       3007.45   7.526     73
       2981.81   7.462     35
       2979.98   7.457     48
       2978.03   7.452    169
       2977.29   7.450    319
       2976.32   7.448    521
       2975.22   7.445    264
       2974.85   7.444    281
       2973.39   7.440    254
       2971.07   7.435    217
       2970.70   7.434    230
       2969.12   7.430   1000
       2967.65   7.426    734
       2965.45   7.421    428
       2962.89   7.414    309
       2961.55   7.411    476
       2960.82   7.409    415
       2959.72   7.406    308
       2957.89   7.402    263
       2948.85   7.379     31
       2946.53   7.373    236
       2945.07   7.370    445
       2943.73   7.366    246
       2941.65   7.361     35
       2939.94   7.357    169
       2937.74   7.351    400
       2935.42   7.345    133
       2931.76   7.336    113
       2930.42   7.333    187
       2929.08   7.330    103
       2924.19   7.317    112
       2922.36   7.313    107
       2919.19   7.305    116
       2916.75   7.299    181
       2916.02   7.297    160
       2914.92   7.294    156
       2914.18   7.292    155
       2911.74   7.286    180
       2911.01   7.284    153
       2909.91   7.282    168
       2908.57   7.278    217
       2906.74   7.274    184
       2903.69   7.266    190
       2901.73   7.261    175
       2879.15   7.205    323
       2877.81   7.201    378
       2873.78   7.191     37
       2871.70   7.186    448
       2870.36   7.183    516
       2867.80   7.176     30
       2866.33   7.173     33
       2864.14   7.167    222
       2862.92   7.164    232
       2861.21   7.160    276
       2859.86   7.156    231
       2853.03   7.139    206
       2851.81   7.136    202
       2850.46   7.133    275
       2849.12   7.130    256
       2842.29   7.112    194
       2840.94   7.109    187
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder